Ni₂(CO)4(CH₂(P(C₆H₅)2)2)2

Base Information

Chemical Name:Ni₂(CO)4(CH₂(P(C₆H₅)2)2)2
CAS No.:112896-40-9
Molecular Formula:C₅₄H₄₄Ni₂O₄P₄
Molecular Weight:998.216
Hs Code.:

Ni<sub>2</sub>(CO)4(CH<sub>2</sub>(P(C<sub>6</sub>H<sub>5</sub>)2)2)2

Synonyms:Ni₂(CO)4(CH₂(P(C₆H₅)2)2)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ni₂(CO)4(CH₂(P(C₆H₅)2)2)2

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Technology Process of Ni₂(CO)4(CH₂(P(C₆H₅)2)2)2

There total 7 articles about Ni₂(CO)4(CH₂(P(C₆H₅)2)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: nickel(II) chloride hexahydrate

: 201230-82-2
carbon monoxide

: 2071-20-7
bis-diphenylphosphinomethane

: 112896-40-9
Ni₂(CO)4(CH₂(P(C₆H₅)2)2)2

Guidance literature:: With sodium tetrahydroborate; In methanol; addn. of equimolar amt. of (C6H5)2PCH2P(C6H5)2 in toluene to soln. of (Ni(H2O)6)Cl2 in CH3OH after introduction of CO for 10 min; addn. of NaBH4 over a period of 5 min with vigorous introduction of CO (20 min); addn. of deoxygenated CH3OH;; pptn.; filtering and drying in vac.; elem. anal.;;
DOI:10.1016/S0020-1693(00)85531-0

Reference yield:

: 75790-05-5
Ni(CO)2(HC(P(C₆H₅)2)3)

: 112896-40-9
Ni₂(CO)4(CH₂(P(C₆H₅)2)2)2

Guidance literature:: Multi-step reaction with 2 steps

1: oxygen / benzene; tetrahydrofuran

With oxygen; In tetrahydrofuran; benzene;
DOI:10.1021/ja00215a018