N,N-dimethyl-N'-((4-(2-methyl-3-morpholino-3-thioxopropanoyl)phenyl)sulfonyl)formimidamide

Base Information

Chemical Name:N,N-dimethyl-N'-((4-(2-methyl-3-morpholino-3-thioxopropanoyl)phenyl)sulfonyl)formimidamide
CAS No.:1394373-87-5
Molecular Formula:C₁₇H₂₃N₃O₄S₂
Molecular Weight:397.519
Hs Code.:

Synonyms:N,N-dimethyl-N'-((4-(2-methyl-3-morpholino-3-thioxopropanoyl)phenyl)sulfonyl)formimidamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-dimethyl-N'-((4-(2-methyl-3-morpholino-3-thioxopropanoyl)phenyl)sulfonyl)formimidamide

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Technology Process of N,N-dimethyl-N'-((4-(2-methyl-3-morpholino-3-thioxopropanoyl)phenyl)sulfonyl)formimidamide

There total 3 articles about N,N-dimethyl-N'-((4-(2-methyl-3-morpholino-3-thioxopropanoyl)phenyl)sulfonyl)formimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.3%

: 110-91-8,99108-56-2
morpholine

: 1394373-85-3
N'-((4-(2-(1,3-dithiatan-2-ylidene)propanoyl)phenyl)sulfonyl)-N,N-dimethylformimidamide

: 1394373-87-5
N,N-dimethyl-N'-((4-(2-methyl-3-morpholino-3-thioxopropanoyl)phenyl)sulfonyl)formimidamide

Guidance literature:: In toluene; at 25 - 120 ℃;

Reference yield:

: 1394373-83-1
N,N-dimethyl-N'-((4-propionylphenyl)sulfonyl)formimidamide

: 1394373-87-5
N,N-dimethyl-N'-((4-(2-methyl-3-morpholino-3-thioxopropanoyl)phenyl)sulfonyl)formimidamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

1.2: 0 - 25 °C / Inert atmosphere

1.3: 0 - 20 °C / Inert atmosphere

2.1: toluene / 25 - 120 °C

With potassium tert-butylate; In tetrahydrofuran; toluene;

Reference yield:

: 90610-45-0
4-propanoylbenzene-1-sulfonamide

: 1394373-87-5
N,N-dimethyl-N'-((4-(2-methyl-3-morpholino-3-thioxopropanoyl)phenyl)sulfonyl)formimidamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethyl acetate; N,N-dimethyl-formamide / 4 h / 25 °C

2.1: potassium tert-butylate / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

2.2: 0 - 25 °C / Inert atmosphere

2.3: 0 - 20 °C / Inert atmosphere

3.1: toluene / 25 - 120 °C

With potassium tert-butylate; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; toluene;