N'-((4-(2-(1,3-dithiatan-2-ylidene)propanoyl)phenyl)sulfonyl)-N,N-dimethylformimidamide

Base Information

Chemical Name:N'-((4-(2-(1,3-dithiatan-2-ylidene)propanoyl)phenyl)sulfonyl)-N,N-dimethylformimidamide
CAS No.:1394373-85-3
Molecular Formula:C₁₄H₁₆N₂O₃S₃
Molecular Weight:356.491
Hs Code.:

Synonyms:N'-((4-(2-(1,3-dithiatan-2-ylidene)propanoyl)phenyl)sulfonyl)-N,N-dimethylformimidamide

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Chemical Property of N'-((4-(2-(1,3-dithiatan-2-ylidene)propanoyl)phenyl)sulfonyl)-N,N-dimethylformimidamide

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Technology Process of N'-((4-(2-(1,3-dithiatan-2-ylidene)propanoyl)phenyl)sulfonyl)-N,N-dimethylformimidamide

There total 2 articles about N'-((4-(2-(1,3-dithiatan-2-ylidene)propanoyl)phenyl)sulfonyl)-N,N-dimethylformimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1394373-83-1
N,N-dimethyl-N'-((4-propionylphenyl)sulfonyl)formimidamide

: 74-95-3
1,1-dibromomethane

: 1394373-85-3
N'-((4-(2-(1,3-dithiatan-2-ylidene)propanoyl)phenyl)sulfonyl)-N,N-dimethylformimidamide

Guidance literature:: N,N-dimethyl-N'-((4-propionylphenyl)sulfonyl)formimidamide; With potassium tert-butylate; In tetrahydrofuran; at 0 - 25 ℃; Inert atmosphere;

carbon disulfide; In tetrahydrofuran; at 0 - 25 ℃; Inert atmosphere;

1,1-dibromomethane; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 90610-45-0
4-propanoylbenzene-1-sulfonamide

: 1394373-85-3
N'-((4-(2-(1,3-dithiatan-2-ylidene)propanoyl)phenyl)sulfonyl)-N,N-dimethylformimidamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethyl acetate; N,N-dimethyl-formamide / 4 h / 25 °C

2.1: potassium tert-butylate / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

2.2: 0 - 25 °C / Inert atmosphere

2.3: 0 - 20 °C / Inert atmosphere

With potassium tert-butylate; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide;