(1,1-dimethylethyl)dimethylsilyl 1-methoxy-1-phenylmethyl peroxide

Base Information

Chemical Name:(1,1-dimethylethyl)dimethylsilyl 1-methoxy-1-phenylmethyl peroxide
CAS No.:295357-38-9
Molecular Formula:C₁₄H₂₄O₃Si
Molecular Weight:268.428
Hs Code.:

Synonyms:(1,1-dimethylethyl)dimethylsilyl 1-methoxy-1-phenylmethyl peroxide

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Chemical Property of (1,1-dimethylethyl)dimethylsilyl 1-methoxy-1-phenylmethyl peroxide

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Technology Process of (1,1-dimethylethyl)dimethylsilyl 1-methoxy-1-phenylmethyl peroxide

There total 3 articles about (1,1-dimethylethyl)dimethylsilyl 1-methoxy-1-phenylmethyl peroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4747-15-3
1-(2-methoxyvinyl)benzene

: 295357-38-9
(1,1-dimethylethyl)dimethylsilyl 1-methoxy-1-phenylmethyl peroxide

Guidance literature:: Multi-step reaction with 2 steps

1: O₃; O₂ / methanol; CH₂Cl₂ / -78 °C

2: imidazole / CH₂Cl₂; dimethylformamide

With 1H-imidazole; oxygen; ozone; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo991714z

Reference yield:

: 100-52-7
benzaldehyde

: 295357-38-9
(1,1-dimethylethyl)dimethylsilyl 1-methoxy-1-phenylmethyl peroxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 0.17 h / 0 °C

1.2: 68 percent / tetrahydrofuran / 1 h / 0 °C

2.1: O₃; O₂ / methanol; CH₂Cl₂ / -78 °C

3.1: imidazole / CH₂Cl₂; dimethylformamide

With 1H-imidazole; oxygen; ozone; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo991714z