[2-Chloro-1-(4-chloro-phenyl)-1-hydroxy-ethyl]-phosphonic acid dimethyl ester

Base Information

• Chemical Name: [2-Chloro-1-(4-chloro-phenyl)-1-hydroxy-ethyl]-phosphonic acid dimethyl ester
• CAS No.: 87198-52-5
• Molecular Formula: C₁₀H₁₃Cl₂O₄P
• Molecular Weight: 299.091

Synonyms:[2-Chloro-1-(4-chloro-phenyl)-1-hydroxy-ethyl]-phosphonic acid dimethyl ester

Chemical Property of [2-Chloro-1-(4-chloro-phenyl)-1-hydroxy-ethyl]-phosphonic acid dimethyl ester

Chemical Property:

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Technology Process of [2-Chloro-1-(4-chloro-phenyl)-1-hydroxy-ethyl]-phosphonic acid dimethyl ester

There total 4 articles about [2-Chloro-1-(4-chloro-phenyl)-1-hydroxy-ethyl]-phosphonic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

p-chlorophenacyl chloride (937-20-2) + phosphorous acid trimethyl ester (121-45-9) → [2-Chloro-1-(4-chloro-phenyl)-1-hydroxy-ethyl]-phosphonic acid dimethyl ester (87198-52-5)

Guidance literature:

In methanol; at 26 ℃; for 24h;

Reference yield:

p-chlorophenacyl chloride (937-20-2) + phosphorous acid trimethyl ester (121-45-9) → para-chloroacetophenone (99-91-2) + [2-Chloro-1-(4-chloro-phenyl)-1-hydroxy-ethyl]-phosphonic acid dimethyl ester (87198-52-5) + Phosphoric acid (E)-2-(4-chloro-phenyl)-vinyl ester dimethyl ester

Guidance literature:

In methanol; at 0 ℃; Product distribution;

Reference yield:

2,2-dichloro-1-(4-chlorophenyl)ethanone (5157-57-3) + phosphorous acid trimethyl ester (121-45-9) → Phosphoric acid (Z)-2-chloro-1-(4-chloro-phenyl)-vinyl ester dimethyl ester (87271-92-9) + para-chloroacetophenone (99-91-2) + [2-Chloro-1-(4-chloro-phenyl)-1-hydroxy-ethyl]-phosphonic acid dimethyl ester (87198-52-5) + Phosphoric acid (E)-2-(4-chloro-phenyl)-vinyl ester dimethyl ester + [2,2-Dichloro-1-(4-chloro-phenyl)-1-hydroxy-ethyl]-phosphonic acid dimethyl ester + Phosphoric acid (E)-2-chloro-1-(4-chloro-phenyl)-vinyl ester dimethyl ester

Guidance literature:

In methanol; at 0 ℃; Product distribution; temperature;

upstream raw materials:

p-chlorophenacyl chloride

phosphorous acid trimethyl ester

2,2-dichloro-1-(4-chlorophenyl)ethanone

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