1-[N²-(1,1-dimethylethoxycarbonyl)-N⁶-(phenylmethoxycarbonyl)-L-lysyl]-4-(4-pyridinyl)piperazine

Base Information

• Chemical Name: 1-[N²-(1,1-dimethylethoxycarbonyl)-N⁶-(phenylmethoxycarbonyl)-L-lysyl]-4-(4-pyridinyl)piperazine
• CAS No.: 204692-44-4
• Molecular Formula: C₂₈H₃₉N₅O₅
• Molecular Weight: 525.648

Synonyms:1-[N²-(1,1-dimethylethoxycarbonyl)-N⁶-(phenylmethoxycarbonyl)-L-lysyl]-4-(4-pyridinyl)piperazine

Chemical Property of 1-[N²-(1,1-dimethylethoxycarbonyl)-N⁶-(phenylmethoxycarbonyl)-L-lysyl]-4-(4-pyridinyl)piperazine

Chemical Property:

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Technology Process of 1-[N²-(1,1-dimethylethoxycarbonyl)-N⁶-(phenylmethoxycarbonyl)-L-lysyl]-4-(4-pyridinyl)piperazine

There total 1 articles about 1-[N²-(1,1-dimethylethoxycarbonyl)-N⁶-(phenylmethoxycarbonyl)-L-lysyl]-4-(4-pyridinyl)piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.2%

Boc-Lys(Z)-OH (2389-45-9) + 4-(piperazin-1-yl)pyridine (1008-91-9) → 1-[N2-(1,1-dimethylethoxycarbonyl)-N6-(phenylmethoxycarbonyl)-L-lysyl]-4-(4-pyridinyl)piperazine (204692-44-4)

Guidance literature:

With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 62.0%

1-[N2-(1,1-dimethylethoxycarbonyl)-N6-(phenylmethoxycarbonyl)-L-lysyl]-4-(4-pyridinyl)piperazine (204692-44-4) → 1-[N6-(phenylmethoxycarbonyl)-L-lysyl]-4-(4-pyridinyl)piperazine (204692-58-0)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃;

Reference yield:

1-[N2-(1,1-dimethylethoxycarbonyl)-N6-(phenylmethoxycarbonyl)-L-lysyl]-4-(4-pyridinyl)piperazine (204692-44-4) + sodium hydrogencarbonate (144-55-8) → 1-[N6-(phenylmethoxycarbonyl)-L-lysyl]-4-(4-pyridinyl)piperazine (204692-58-0)

Guidance literature:

With trifluoroacetic acid; In dichloromethane;

upstream raw materials:

Boc-Lys(Z)-OH

4-(piperazin-1-yl)pyridine

Downstream raw materials:

1-[N⁶-(phenylmethoxycarbonyl)-L-lysyl]-4-(4-pyridinyl)piperazine

1-[N²-(3,5-dibromo-D-tyrosyl)-N⁶-(phenylmethoxycarbonyl)-L-lysyl]-4-(4-pyridinyl)piperazine

1-[N₂-[N-(1,1-dimethylethoxycarbonyl)-3,5-dibromo-D-tyrosyl]-N₆-(phenylmethoxycarbonyl)-L-lysyl]-4-(4-pyridinyl)-piperazine

1-[N²-[3,5-dibromo-N-[[[2-(2-methoxyphenyl)ethyl]-amino]carbonyl]-D-tyrosyl]-N⁶-(phenylmethoxycarbonyl)-L-lysyl]-4-(4-pyridinyl)piperazine

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