[(S)-2-(3,4-dimethoxyphenyl)-1-methylcarbamoyl-ethyl]carbamic acid tert-butyl ester

Base Information

Chemical Name:[(S)-2-(3,4-dimethoxyphenyl)-1-methylcarbamoyl-ethyl]carbamic acid tert-butyl ester
CAS No.:944416-22-2
Molecular Formula:C₁₇H₂₆N₂O₅
Molecular Weight:338.404
Hs Code.:

Synonyms:[(S)-2-(3,4-dimethoxyphenyl)-1-methylcarbamoyl-ethyl]carbamic acid tert-butyl ester

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Chemical Property of [(S)-2-(3,4-dimethoxyphenyl)-1-methylcarbamoyl-ethyl]carbamic acid tert-butyl ester

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Technology Process of [(S)-2-(3,4-dimethoxyphenyl)-1-methylcarbamoyl-ethyl]carbamic acid tert-butyl ester

There total 1 articles about [(S)-2-(3,4-dimethoxyphenyl)-1-methylcarbamoyl-ethyl]carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 138908-56-2
(S)-(+)-2-tert-butoxycarbonylamino-3-(3,4-dimethoxyphenyl)propionic acid methyl ester

: 74-89-5
methylamine

: 944416-22-2
[(S)-2-(3,4-dimethoxyphenyl)-1-methylcarbamoyl-ethyl]carbamic acid tert-butyl ester

Guidance literature:: In methanol; water; at 20 ℃; for 4h;
DOI:10.1016/j.tet.2007.04.024

Reference yield:

: 944416-22-2
[(S)-2-(3,4-dimethoxyphenyl)-1-methylcarbamoyl-ethyl]carbamic acid tert-butyl ester

: 944416-37-9
(S)-2-amino-3-(3,4-dimethoxyphenyl)-N-methyl-propionamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1016/j.tet.2007.04.024

Reference yield:

: 944416-22-2
[(S)-2-(3,4-dimethoxyphenyl)-1-methylcarbamoyl-ethyl]carbamic acid tert-butyl ester

: 944416-23-3
[(S)-1-((1R,3S)-6,7-dimethoxy-3-methylcarbamoyl-1,2,3,4-tetrahydroisoquinolin-1-yl)ethyl]carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: TFA / CH₂Cl₂ / 3 h / 0 °C

2: 126 mg / TFA / CH₂Cl₂ / 12 h / 20 °C

With trifluoroacetic acid; In dichloromethane; 2: Pictet-Spengler condensation;
DOI:10.1016/j.tet.2007.04.024