ethyl 1-<3,4-bis(benzyloxy)phenyl>iminoacetate hydrochloride

Base Information

• Chemical Name: ethyl 1-<3,4-bis(benzyloxy)phenyl>iminoacetate hydrochloride
• CAS No.: 85612-50-6
• Molecular Formula: C₂₄H₂₅NO₃*ClH
• Molecular Weight: 411.928
• Mol file: 85612-50-6.mol

Synonyms:ethyl 1-<3,4-bis(benzyloxy)phenyl>iminoacetate hydrochloride

Chemical Property of ethyl 1-<3,4-bis(benzyloxy)phenyl>iminoacetate hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl 1-<3,4-bis(benzyloxy)phenyl>iminoacetate hydrochloride

There total 1 articles about ethyl 1-<3,4-bis(benzyloxy)phenyl>iminoacetate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

ethanol (64-17-5) + (3,4-bis-benzyloxyphenyl)acetonitrile (1699-60-1) → ethyl 1-<3,4-bis(benzyloxy)phenyl>iminoacetate hydrochloride (85612-50-6)

Guidance literature:

With hydrogenchloride; In benzene; at 0 ℃;

DOI:10.1021/jm00361a005

Reference yield: 95.0%

ethyl 1-<3,4-bis(benzyloxy)phenyl>iminoacetate hydrochloride (85612-50-6) + N-methyl-ethane-1,2-diamine (109-81-9) → 1-methyl-2-<3,4-bis(benzyloxy)benzyl>imidazoline (85612-51-7)

Guidance literature:

In dichloromethane; for 4h; Ambient temperature;

DOI:10.1021/jm00361a005

Reference yield: 92.9%

ethyl 1-<3,4-bis(benzyloxy)phenyl>iminoacetate hydrochloride (85612-50-6) + ethylenediamine (107-15-3,85404-18-8) → 2-<3,4-bis(benzyloxy)benzyl>imidazoline (85612-49-3)

Guidance literature:

In dichloromethane; for 15h; Ambient temperature;

DOI:10.1021/jm00361a005

upstream raw materials:

ethanol

(3,4-bis-benzyloxyphenyl)acetonitrile

Downstream raw materials:

(S)-2-(3,4-Bis-benzyloxy-benzyl)-4-methyl-4,5-dihydro-1H-imidazole

(R)-2-(3,4-Bis-benzyloxy-benzyl)-4-methyl-4,5-dihydro-1H-imidazole

(S)-4-Benzyl-2-(3,4-bis-benzyloxy-benzyl)-4,5-dihydro-1H-imidazole

(R)-4-Benzyl-2-(3,4-bis-benzyloxy-benzyl)-4,5-dihydro-1H-imidazole