3,5-bis[N-(3-chlorophenyl)carbamoyl]-2,6-dimethylpyridine

Base Information

Chemical Name:3,5-bis[N-(3-chlorophenyl)carbamoyl]-2,6-dimethylpyridine
CAS No.:1354571-19-9
Molecular Formula:C₂₁H₁₇Cl₂N₃O₂
Molecular Weight:414.291
Hs Code.:

Synonyms:3,5-bis[N-(3-chlorophenyl)carbamoyl]-2,6-dimethylpyridine

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Chemical Property of 3,5-bis[N-(3-chlorophenyl)carbamoyl]-2,6-dimethylpyridine

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Technology Process of 3,5-bis[N-(3-chlorophenyl)carbamoyl]-2,6-dimethylpyridine

There total 4 articles about 3,5-bis[N-(3-chlorophenyl)carbamoyl]-2,6-dimethylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1354571-13-3
3,5-bis(3',5'-dimethyl-1'-pyrazolylcarbonyl)-2,6-dimethylpyridine

: 108-42-9
3-chloro-aniline

: 1354571-19-9
3,5-bis[N-(3-chlorophenyl)carbamoyl]-2,6-dimethylpyridine

Guidance literature:: With acetic acid; In toluene; for 1h; Reflux;
DOI:10.1002/cjoc.201180367

Reference yield:

: 1149-24-2
2,6-dimethyl-pyridine-3,5-dicarboxylic acid diethyl ester

: 1354571-19-9
3,5-bis[N-(3-chlorophenyl)carbamoyl]-2,6-dimethylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / 6 h / Reflux; Neat (no solvent)

2: toluene-4-sulfonic acid / chloroform / 2 h / Reflux

3: acetic acid / toluene / 1 h / Reflux

With toluene-4-sulfonic acid; hydrazine hydrate; acetic acid; In chloroform; toluene;
DOI:10.1002/cjoc.201180367

Reference yield:

: 1149-23-1
diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate

: 1354571-19-9
3,5-bis[N-(3-chlorophenyl)carbamoyl]-2,6-dimethylpyridine

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; sodium nitrite / ethanol; water / 1 h / Reflux

2: hydrazine hydrate / 6 h / Reflux; Neat (no solvent)

3: toluene-4-sulfonic acid / chloroform / 2 h / Reflux

4: acetic acid / toluene / 1 h / Reflux

With toluene-4-sulfonic acid; hydrazine hydrate; acetic acid; sodium nitrite; In ethanol; chloroform; water; toluene;
DOI:10.1002/cjoc.201180367