Quinoline, 1,2-dihydro-1-methyl-2-methylene-(8CI,9CI)

Base Information

Chemical Name:Quinoline, 1,2-dihydro-1-methyl-2-methylene-(8CI,9CI)
CAS No.:16782-09-5
Molecular Formula:C₁₁H₁₁N
Molecular Weight:157.215
Hs Code.:2933499090
DSSTox Substance ID:DTXSID40450762
Mol file:16782-09-5.mol

Synonyms:16782-09-5;Quinoline, 1,2-dihydro-1-methyl-2-methylene- (8CI,9CI);1-METHYL-2-METHYLIDENEQUINOLINE;1-Methyl-2-methylene-1,2-dihydroquinoline;1-methyl-2-methylidene-1,2-dihydroquinoline;1,2-dihydro-1-methyl-2-methylene-quinoline;Quinoline,1,2-dihydro-1-methyl-2-methylene-(8CI,9CI);SCHEMBL10105334;DTXSID40450762;WIKKZOOWSULEGM-UHFFFAOYSA-N;Quinoline, 1,2-dihydro-1-methyl-2-methylene-

Suppliers and Price of Quinoline, 1,2-dihydro-1-methyl-2-methylene-(8CI,9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Quinoline, 1,2-dihydro-1-methyl-2-methylene-(8CI,9CI)

Chemical Property:

Melting Point:71-72 °C
Boiling Point:257.1±23.0 °C(Predicted)
PKA:1.68±0.20(Predicted)
PSA：4.93000
Density:1.06±0.1 g/cm3(Predicted)
LogP:1.86970
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:157.089149355
Heavy Atom Count:12
Complexity:217

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C(=C)C=CC2=CC=CC=C21

Technology Process of Quinoline, 1,2-dihydro-1-methyl-2-methylene-(8CI,9CI)

There total 7 articles about Quinoline, 1,2-dihydro-1-methyl-2-methylene-(8CI,9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 876-87-9
N-methylquinaldinium iodide

: 16782-09-5
1-methyl-2-methylene-1,2-dihydro-quinoline

Guidance literature:: With sodium hydroxide;
DOI:10.1007/BF00475576

Reference yield:

: 1,2-dimethylquinolinium hexafluorophosphate

: 16782-09-5
1-methyl-2-methylene-1,2-dihydro-quinoline

Guidance literature:: With potassium hydride; In tetrahydrofuran-d8; for 1h;
DOI:10.1002/(SICI)1099-0690(200002)2000:3<507::AID-EJOC507<3.0.CO;2-V

Reference yield:

: 91-63-4
2-methylquinoline

: 16782-09-5
1-methyl-2-methylene-1,2-dihydro-quinoline

Guidance literature:: Multi-step reaction with 2 steps

2: KOH / H₂O; toluene

With potassium hydroxide; In water; toluene;
DOI:10.1007/BF00811679