C₃₃H₃₆N₂O₇S₂

Base Information

Chemical Name:C₃₃H₃₆N₂O₇S₂
CAS No.:1312018-09-9
Molecular Formula:C₃₃H₃₆N₂O₇S₂
Molecular Weight:636.79
Hs Code.:

C<sub>33</sub>H<sub>36</sub>N<sub>2</sub>O<sub>7</sub>S<sub>2</sub>

Synonyms:C₃₃H₃₆N₂O₇S₂

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Chemical Property of C₃₃H₃₆N₂O₇S₂

Chemical Property:

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Technology Process of C₃₃H₃₆N₂O₇S₂

There total 14 articles about C₃₃H₃₆N₂O₇S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1312018-08-8
1-[1-benzenesulfonyl-5-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl)-1H-pyrrolo[2,3-b]pyridin-2-yl]-2-cyclopentyl-ethanone

: 4124-41-8
p-toluenesulfonylanhydride

: 1312018-09-9
C₃₃H₃₆N₂O₇S₂

Guidance literature:: 1-[1-benzenesulfonyl-5-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl)-1H-pyrrolo[2,3-b]pyridin-2-yl]-2-cyclopentyl-ethanone; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h;

p-toluenesulfonylanhydride; In tetrahydrofuran; at -78 ℃; for 1.5h; Product distribution / selectivity;

Reference yield:

: 271-63-6
7-Azaindole

: 1312018-09-9
C₃₃H₃₆N₂O₇S₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: triethylamine; formic acid / palladium 10% on activated carbon / 120 h / 0 - 80 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

2.2: 3 h / 0 °C

3.1: bromine; pyridine / dichloromethane / 2 h / 0 °C

4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h

5.1: sodium hydroxide; tetrabutylammomium bromide / dichloromethane / 0.08 h / 0 °C

5.2: 12.25 h / 0 - 25 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 12 h / 20 - 80 °C

7.1: 1,4-bis(9-O-dihydroquinidine)phthalazine; methanesulfonamide / water; tert-butyl alcohol / 12 h / 0 °C

7.2: 0.5 h / 25 °C

8.1: toluene-4-sulfonic acid / dichloromethane / 12 h / 25 °C

9.1: lithium diisopropyl amide / tetrahydrofuran / 0.08 h / -78 °C

9.2: 1 h / -78 °C

10.1: Dess-Martin periodane / dichloromethane / 1 h / 25 °C

11.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

11.2: 1.5 h / -78 °C

With pyridine; formic acid; methanesulfonamide; tetrabutylammomium bromide; bromine; sodium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; lithium hexamethyldisilazane; lithium diisopropyl amide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; tert-butyl alcohol;

Reference yield:

: 1-(tert-butyl-dimethyl-silanyl)-2,3-dihydro-1H-pyrrolo[2,3-b]pyridine

: 1312018-09-9
C₃₃H₃₆N₂O₇S₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: bromine; pyridine / dichloromethane / 2 h / 0 °C

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h

3.1: sodium hydroxide; tetrabutylammomium bromide / dichloromethane / 0.08 h / 0 °C

3.2: 12.25 h / 0 - 25 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 12 h / 20 - 80 °C

5.1: 1,4-bis(9-O-dihydroquinidine)phthalazine; methanesulfonamide / water; tert-butyl alcohol / 12 h / 0 °C

5.2: 0.5 h / 25 °C

6.1: toluene-4-sulfonic acid / dichloromethane / 12 h / 25 °C

7.1: lithium diisopropyl amide / tetrahydrofuran / 0.08 h / -78 °C

7.2: 1 h / -78 °C

8.1: Dess-Martin periodane / dichloromethane / 1 h / 25 °C

9.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

9.2: 1.5 h / -78 °C

With pyridine; methanesulfonamide; tetrabutylammomium bromide; bromine; Dess-Martin periodane; toluene-4-sulfonic acid; 1,4-bis(9-O-dihydroquinidine)phthalazine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; lithium hexamethyldisilazane; lithium diisopropyl amide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;