[(1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazin-7-yl)sulfanyl]methyl cyanide

Base Information

Chemical Name:[(1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazin-7-yl)sulfanyl]methyl cyanide
CAS No.:1254940-16-3
Molecular Formula:C₁₆H₁₃N₇OS
Molecular Weight:351.392
Hs Code.:

Synonyms:[(1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazin-7-yl)sulfanyl]methyl cyanide

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Chemical Property of [(1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazin-7-yl)sulfanyl]methyl cyanide

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Technology Process of [(1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazin-7-yl)sulfanyl]methyl cyanide

There total 5 articles about [(1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazin-7-yl)sulfanyl]methyl cyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1254940-03-8
1,5-dimethyl-3-phenyl-7,8-dihydro-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazine-7-thione

: 1254940-16-3
[(1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazin-7-yl)sulfanyl]methyl cyanide

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; acetonitrile; for 4h; Reflux;
DOI:10.3184/030823410X520778

Reference yield:

: C₁₄H₁₂N₆OS

: 107-14-2
chloroacetonitrile

: 1254940-16-3
[(1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazin-7-yl)sulfanyl]methyl cyanide

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; acetonitrile; for 4h; Heating;
DOI:10.1134/S1068162015020077

Reference yield:

: 98-88-4
benzoyl chloride

: 1254940-16-3
[(1,5-dimethyl-3-phenyl-1H-[1,2,4]triazolo[4',3':1,2]pyrimido[4,5-e][1,3,4]oxadiazin-7-yl)sulfanyl]methyl cyanide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile

2: hydrazine hydrate / ethanol / 120 h / Reflux

3: pyridine / 6 h / Reflux

4: triethylamine / acetonitrile; N,N-dimethyl-formamide / 4 h / Heating

With pyridine; potassium carbonate; hydrazine hydrate; triethylamine; In ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1134/S1068162015020077