α-<2-amino>ethyl>-p-nitrobenzyl alcohol

Base Information

Chemical Name:α-<2-amino>ethyl>-p-nitrobenzyl alcohol
CAS No.:136247-26-2
Molecular Formula:C₁₈H₂₂N₂O₅
Molecular Weight:346.383
Hs Code.:

α-<2-<N-<2-(3,4-dimethoxyphenyl)ethyl>amino>ethyl>-p-nitrobenzyl alcohol

Synonyms:α-<2-amino>ethyl>-p-nitrobenzyl alcohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-<2-amino>ethyl>-p-nitrobenzyl alcohol

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Technology Process of α-<2-amino>ethyl>-p-nitrobenzyl alcohol

There total 3 articles about α-<2-amino>ethyl>-p-nitrobenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 6388-74-5,38201-14-8,71884-55-4
p-Nitrophenyloxirane

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 136247-26-2
α-<2-amino>ethyl>-p-nitrobenzyl alcohol

Guidance literature:: In tetrahydrofuran; at 20 ℃; Inert atmosphere; Reflux;
DOI:10.1038/aps.2012.151

Reference yield:

: 99-81-0
4-Nitrophenacyl bromide

: 136247-26-2
α-<2-amino>ethyl>-p-nitrobenzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; sodium tetrahydroborate / tetrahydrofuran; methanol / 0.58 h / 0 - 20 °C

2: tetrahydrofuran / 20 °C / Inert atmosphere; Reflux

With sodium tetrahydroborate; sodium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1038/aps.2012.151

Reference yield:

: 100-19-6
(4-nitrophenyl)ethanone

: 136247-26-2
α-<2-amino>ethyl>-p-nitrobenzyl alcohol

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride; bromine / diethyl ether / 3 h / 0 - 20 °C

2: sodium hydroxide; sodium tetrahydroborate / tetrahydrofuran; methanol / 0.58 h / 0 - 20 °C

3: tetrahydrofuran / 20 °C / Inert atmosphere; Reflux

With aluminum (III) chloride; sodium tetrahydroborate; bromine; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1038/aps.2012.151