In₂Br₄(N,N,N',N'-tetramethylethylenediamine)2

Base Information

Chemical Name:In₂Br₄(N,N,N',N'-tetramethylethylenediamine)2
CAS No.:81985-78-6
Molecular Formula:C₁₂H₃₂Br₄In₂N₄
Molecular Weight:781.669
Hs Code.:

In<sub>2</sub>Br<sub>4</sub>(N,N,N',N'-tetramethylethylenediamine)2

Synonyms:In₂Br₄(N,N,N',N'-tetramethylethylenediamine)2

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Chemical Property of In₂Br₄(N,N,N',N'-tetramethylethylenediamine)2

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Technology Process of In₂Br₄(N,N,N',N'-tetramethylethylenediamine)2

There total 2 articles about In₂Br₄(N,N,N',N'-tetramethylethylenediamine)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: indium(I) bromide

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 7440-74-6
indium

: 81985-78-6
In₂Br₄(N,N,N',N'-tetramethylethylenediamine)2

Guidance literature:: In toluene; InBr powder suspnd. on 10% v/v tmeda/toluene at -85°C, warmed above -20°C;
DOI:10.1039/b814658f

Reference yield:

: indium(II) bromide

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 81985-78-6
In₂Br₄(N,N,N',N'-tetramethylethylenediamine)2

: In₂Br₄((CH₃)2NCH₂CH₂N(CH₃)2)2*C₆H₆

Guidance literature:: With benzene; In benzene; addn. of ligand at -195.8°C under N2 in the minimum amount of solvent, then the cooling bath was removed, and the system was stirred for 20 min after the solvent had completely melted; the suspension was filtered, and the solid collected and dried yielding solvent-free complex, mother liquor allowed to stand 72 h, crystn. of In2Br4(TMED)2C6H6; elem. anal.;
DOI:10.1139/v82-101

Reference yield: 34.0%

: 81985-78-6
In₂Br₄(N,N,N',N'-tetramethylethylenediamine)2

: 108894-99-1
(2,4,6-triisopropylphenyl)magnesium bromide

: 184002-14-0
In₂(C₆H₂(C₃H₇)3)4

Guidance literature:: In diethyl ether; (anaerobic and anhydrous conditions); addn. of the Grignard compd. in Et2O to the In complex in Et2O at -78°C, stirring 1 h at this temp., warming to -15°C, stirring several h at this temp.; removal of solvent (reduced pressure, -10°C), extn. (hexane, -10°C), concn., crystn. on cooling to -20°C;
DOI:10.1002/anie.199623551