(S)-2-Amino-N-((1S,2R)-2-benzyloxy-1-{(S)-1-[(1S,2R)-2-benzyloxy-1-(2-dimethylamino-ethylcarbamoyl)-propylcarbamoyl]-2-methyl-propylcarbamoyl}-propyl)-3-methyl-butyramide

Base Information

• Chemical Name: (S)-2-Amino-N-((1S,2R)-2-benzyloxy-1-{(S)-1-[(1S,2R)-2-benzyloxy-1-(2-dimethylamino-ethylcarbamoyl)-propylcarbamoyl]-2-methyl-propylcarbamoyl}-propyl)-3-methyl-butyramide
• CAS No.: 287957-59-9
• Molecular Formula: C₃₆H₅₆N₆O₆
• Molecular Weight: 668.877

Synonyms:(S)-2-Amino-N-((1S,2R)-2-benzyloxy-1-{(S)-1-[(1S,2R)-2-benzyloxy-1-(2-dimethylamino-ethylcarbamoyl)-propylcarbamoyl]-2-methyl-propylcarbamoyl}-propyl)-3-methyl-butyramide

Chemical Property of (S)-2-Amino-N-((1S,2R)-2-benzyloxy-1-{(S)-1-[(1S,2R)-2-benzyloxy-1-(2-dimethylamino-ethylcarbamoyl)-propylcarbamoyl]-2-methyl-propylcarbamoyl}-propyl)-3-methyl-butyramide

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Technology Process of (S)-2-Amino-N-((1S,2R)-2-benzyloxy-1-{(S)-1-[(1S,2R)-2-benzyloxy-1-(2-dimethylamino-ethylcarbamoyl)-propylcarbamoyl]-2-methyl-propylcarbamoyl}-propyl)-3-methyl-butyramide

There total 3 articles about (S)-2-Amino-N-((1S,2R)-2-benzyloxy-1-{(S)-1-[(1S,2R)-2-benzyloxy-1-(2-dimethylamino-ethylcarbamoyl)-propylcarbamoyl]-2-methyl-propylcarbamoyl}-propyl)-3-methyl-butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Boc-Val-Thr(bzl)-Val-Thr(bzl)-dmda (858099-76-0) → (S)-2-Amino-N-((1S,2R)-2-benzyloxy-1-{(S)-1-[(1S,2R)-2-benzyloxy-1-(2-dimethylamino-ethylcarbamoyl)-propylcarbamoyl]-2-methyl-propylcarbamoyl}-propyl)-3-methyl-butyramide (287957-59-9)

Guidance literature:

With trifluoroacetic acid; In dichloromethane;

DOI:10.1021/ja050558c

Reference yield:

t-Boc-L-valine (13734-41-3) → (S)-2-Amino-N-((1S,2R)-2-benzyloxy-1-{(S)-1-[(1S,2R)-2-benzyloxy-1-(2-dimethylamino-ethylcarbamoyl)-propylcarbamoyl]-2-methyl-propylcarbamoyl}-propyl)-3-methyl-butyramide (287957-59-9)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. TFA / CH₂Cl₂

With trifluoroacetic acid; In dichloromethane;

DOI:10.1021/ja050558c

Reference yield:

N-Boc-O-benzyl-L-threonine (15260-10-3) → (S)-2-Amino-N-((1S,2R)-2-benzyloxy-1-{(S)-1-[(1S,2R)-2-benzyloxy-1-(2-dimethylamino-ethylcarbamoyl)-propylcarbamoyl]-2-methyl-propylcarbamoyl}-propyl)-3-methyl-butyramide (287957-59-9)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. TFA / CH₂Cl₂

With trifluoroacetic acid; In dichloromethane;

DOI:10.1021/ja050558c

upstream raw materials:

Boc-Val-Thr(bzl)-Val-Thr(bzl)-dmda

t-Boc-L-valine

N-Boc-O-benzyl-L-threonine

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