O-(tert-butyldiphenylsilyloxy-2-quinolyl)methyl-N,N'-dicyclohexylisourea

Base Information

Chemical Name:O-(tert-butyldiphenylsilyloxy-2-quinolyl)methyl-N,N'-dicyclohexylisourea
CAS No.:168204-20-4
Molecular Formula:C₃₉H₄₉N₃O₂Si
Molecular Weight:619.922
Hs Code.:

Synonyms:O-(tert-butyldiphenylsilyloxy-2-quinolyl)methyl-N,N'-dicyclohexylisourea

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Chemical Property of O-(tert-butyldiphenylsilyloxy-2-quinolyl)methyl-N,N'-dicyclohexylisourea

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Technology Process of O-(tert-butyldiphenylsilyloxy-2-quinolyl)methyl-N,N'-dicyclohexylisourea

There total 5 articles about O-(tert-butyldiphenylsilyloxy-2-quinolyl)methyl-N,N'-dicyclohexylisourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.4%

: 538-75-0
dicyclohexyl-carbodiimide

: 155933-77-0
<8-<(tert-butyldiphenylsilyl)oxy>quinolyl>methanol

: 168204-20-4
O-(tert-butyldiphenylsilyloxy-2-quinolyl)methyl-N,N'-dicyclohexylisourea

Guidance literature:: With copper(l) chloride; 1.) 50 deg C, 1 h, 2.) RT, 24 h;
DOI:10.1021/ja00133a013

Reference yield:

: 826-81-3
2-methyl-8-quinolinol

: 168204-20-4
O-(tert-butyldiphenylsilyloxy-2-quinolyl)methyl-N,N'-dicyclohexylisourea

Guidance literature:: Multi-step reaction with 4 steps

1: 84.1 percent / imidazole / dimethylformamide / 72 h / Ambient temperature

2: 76.7 percent / SeO₂ / dioxane / 24 h / 75 °C

3: 93.8 percent / NaBH₄ / ethanol / 6 h / Ambient temperature

4: 88.4 percent / CuCl / 1.) 50 deg C, 1 h, 2.) RT, 24 h

With 1H-imidazole; sodium tetrahydroborate; selenium(IV) oxide; copper(l) chloride; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja00133a013

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 168204-20-4
O-(tert-butyldiphenylsilyloxy-2-quinolyl)methyl-N,N'-dicyclohexylisourea

Guidance literature:: Multi-step reaction with 4 steps

1: 84.1 percent / imidazole / dimethylformamide / 72 h / Ambient temperature

2: 76.7 percent / SeO₂ / dioxane / 24 h / 75 °C

3: 93.8 percent / NaBH₄ / ethanol / 6 h / Ambient temperature

4: 88.4 percent / CuCl / 1.) 50 deg C, 1 h, 2.) RT, 24 h

With 1H-imidazole; sodium tetrahydroborate; selenium(IV) oxide; copper(l) chloride; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja00133a013