2-fluoro-5-(2-methyl-6-(3-(methylsulfonyl)propoxy)pyridin-3-yl)benzaldehyde

Base Information

Chemical Name:2-fluoro-5-(2-methyl-6-(3-(methylsulfonyl)propoxy)pyridin-3-yl)benzaldehyde
CAS No.:1544740-75-1
Molecular Formula:C₁₇H₁₈FNO₄S
Molecular Weight:351.399
Hs Code.:

Synonyms:2-fluoro-5-(2-methyl-6-(3-(methylsulfonyl)propoxy)pyridin-3-yl)benzaldehyde

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Chemical Property of 2-fluoro-5-(2-methyl-6-(3-(methylsulfonyl)propoxy)pyridin-3-yl)benzaldehyde

Chemical Property:

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Technology Process of 2-fluoro-5-(2-methyl-6-(3-(methylsulfonyl)propoxy)pyridin-3-yl)benzaldehyde

There total 1 articles about 2-fluoro-5-(2-methyl-6-(3-(methylsulfonyl)propoxy)pyridin-3-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1544740-76-2
C₁₇H₂₀FNO₄S

: 1544740-75-1
2-fluoro-5-(2-methyl-6-(3-(methylsulfonyl)propoxy)pyridin-3-yl)benzaldehyde

Guidance literature:: With manganese(IV) oxide; In tetrahydrofuran; at 60 ℃; for 1h;

Reference yield:

: 1544739-15-2
4-amino-1,1a,6,6a-tetrahydro-3-aza-cyclopropa[a]indene-1-carboxylic acid ethyl ester

: 1544740-75-1
2-fluoro-5-(2-methyl-6-(3-(methylsulfonyl)propoxy)pyridin-3-yl)benzaldehyde

: 1544740-77-3
ethyl 3-((2-fluoro-5-(2-methyl-6-(3-(methylsulfonyl)propoxy)pyridin-3-yl)benzyl)amino)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

Guidance literature:: 4-amino-1,1a,6,6a-tetrahydro-3-aza-cyclopropa[a]indene-1-carboxylic acid ethyl ester; 2-fluoro-5-(2-methyl-6-(3-(methylsulfonyl)propoxy)pyridin-3-yl)benzaldehyde; With titanium tetrachloride; triethylamine; In dichloromethane; at -40 - 20 ℃; for 16h;

With sodium tris(acetoxy)borohydride; In ethanol; at 20 ℃; for 1h;

Reference yield:

: 1544740-75-1
2-fluoro-5-(2-methyl-6-(3-(methylsulfonyl)propoxy)pyridin-3-yl)benzaldehyde

: 1544740-74-0
3-((2-fluoro-5-(2-methyl-6-(3-(methylsulfonyl)propoxy)pyridin-3-yl)benzyl)amino)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium tetrachloride; triethylamine / dichloromethane / 16 h / -40 - 20 °C

1.2: 1 h / 20 °C

2.1: water; lithium hydroxide / tetrahydrofuran; ethanol / 20 °C

With water; titanium tetrachloride; triethylamine; lithium hydroxide; In tetrahydrofuran; ethanol; dichloromethane;