[(3aS,4S,6R,6aS)-6-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl][(1-methoxyphenyl)meth-(Z)-ylidene]amine N-oxide

Base Information

Chemical Name:[(3aS,4S,6R,6aS)-6-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl][(1-methoxyphenyl)meth-(Z)-ylidene]amine N-oxide
CAS No.:86467-68-7
Molecular Formula:C₂₀H₂₇NO₇
Molecular Weight:393.437
Hs Code.:

Synonyms:[(3aS,4S,6R,6aS)-6-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl][(1-methoxyphenyl)meth-(Z)-ylidene]amine N-oxide

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Chemical Property of [(3aS,4S,6R,6aS)-6-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl][(1-methoxyphenyl)meth-(Z)-ylidene]amine N-oxide

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Technology Process of [(3aS,4S,6R,6aS)-6-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl][(1-methoxyphenyl)meth-(Z)-ylidene]amine N-oxide

There total 1 articles about [(3aS,4S,6R,6aS)-6-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl][(1-methoxyphenyl)meth-(Z)-ylidene]amine N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 35023-80-4
2,3:5,6-di-O-isopropylidene-D-mannose oxime

: 123-11-5
4-methoxy-benzaldehyde

: 86467-68-7
[(3aS,4S,6R,6aS)-6-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl][(1-methoxyphenyl)meth-(Z)-ylidene]amine N-oxide

Guidance literature:: In toluene; for 16h; Heating;
DOI:10.1002/anie.200461934

Reference yield: 76.0%

: 3173-56-6
benzyl isothiocyanate

: 86467-68-7
[(3aS,4S,6R,6aS)-6-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl][(1-methoxyphenyl)meth-(Z)-ylidene]amine N-oxide

: 849441-29-8
(R)-4-benzyl-2-[(3aS,4S,6R,6aS)-6-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl]-3-(4-methoxyphenyl)-1,2,4-oxadiazolidin-5-one

: (S)-4-benzyl-2-[(3aS,4S,6R,6aS)-6-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl]-3-(4-methoxyphenyl)-1,2,4-oxadiazolidin-5-one

Guidance literature:: In dichloromethane; for 40h; Heating;
DOI:10.1002/anie.200461934

Reference yield:

: 86467-68-7
[(3aS,4S,6R,6aS)-6-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl][(1-methoxyphenyl)meth-(Z)-ylidene]amine N-oxide

: (R)-4-benzyl-3-(4-methoxyphenyl)-1,2,4-oxadiazolidin-5-one

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / CH₂Cl₂ / 40 h / Heating

2: 88 percent / 4-toluenesulfonic acid hydrate / methanol; H₂O / 2 h / Heating

With p-toluenesulfonic acid monohydrate; In methanol; dichloromethane; water;
DOI:10.1002/anie.200461934