C₆₁H₇₂N₂O₁₃Si

Base Information

Chemical Name:C₆₁H₇₂N₂O₁₃Si
CAS No.:1383446-52-3
Molecular Formula:C₆₁H₇₂N₂O₁₃Si
Molecular Weight:1069.33
Hs Code.:

C<sub>61</sub>H<sub>72</sub>N<sub>2</sub>O<sub>13</sub>Si

Synonyms:C₆₁H₇₂N₂O₁₃Si

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Chemical Property of C₆₁H₇₂N₂O₁₃Si

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Technology Process of C₆₁H₇₂N₂O₁₃Si

There total 1 articles about C₆₁H₇₂N₂O₁₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1383446-50-1
C₅₉H₆₈N₄O₁₂Si

: 507-09-5
tiolacetic acid

: 1383446-52-3
C₆₁H₇₂N₂O₁₃Si

Guidance literature:: In pyridine; at 20 ℃; for 48h;
DOI:10.1016/j.carres.2012.04.010

Reference yield: 93.0%

: 1383446-52-3
C₆₁H₇₂N₂O₁₃Si

: 121-44-8
triethylamine

: 2C₆H₁₅N*C₆₁H₇₂N₂O₁₉S₂Si

Guidance literature:: C₆₁H₇₂N₂O₁₃Si; With sulfur trioxide trimethylamine complex; In N,N-dimethyl-formamide; at 55 ℃; for 10h;

triethylamine; In methanol; chloroform; solid phase reaction;
DOI:10.1016/j.carres.2012.04.010

Reference yield:

: 1383446-52-3
C₆₁H₇₂N₂O₁₃Si

: C₄₅H₅₁N₂O₂₂S₃^(3-)*3Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfur trioxide trimethylamine complex / N,N-dimethyl-formamide / 10 h / 55 °C

1.2: solid phase reaction

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / 48 h / 20 °C

3.1: magnesium bromide diethyl etherate / diethyl ether; nitromethane / 10 h / 20 °C

4.1: pyridine / 40 h / 20 °C

5.1: sulfur trioxide pyridine complex; triethylamine / pyridine / 1 h / 70 °C / Microwave irradiation

6.1: sodium hydroxide / methanol; water / solid phase reaction

With magnesium bromide diethyl etherate; tetrabutyl ammonium fluoride; sulfur trioxide trimethylamine complex; sulfur trioxide pyridine complex; triethylamine; sodium hydroxide; In tetrahydrofuran; pyridine; methanol; diethyl ether; nitromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2012.04.010