Phosphorusnitriledichloridetrimer

Base Information

• Chemical Name: Phosphorusnitriledichloridetrimer
• CAS No.: 16422-79-0
• Molecular Formula: Cl₆N₃P₃
• Molecular Weight: 347.659
• Mol file: 16422-79-0.mol

Synonyms:Phosphonitrile chloride, trimer

Chemical Property of Phosphorusnitriledichloridetrimer

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Phosphorusnitriledichloridetrimer

There total 43 articles about Phosphorusnitriledichloridetrimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

phosphorus pentachloride (10026-13-8,874483-75-7) + ammonium chloride (12125-02-9) → 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine (940-71-6,16422-79-0) + (NPCl2)8 (14514-98-8) + octachlorocyclotetraphosphazene (2950-45-0) + Cl18N9P9 + pentakisphosphorus nitride dichloride (13596-41-3) + hexakisphosphorus nitride dichloride (2851-52-7) + heptakisphosphorus nitride dichloride (13827-30-0)

Guidance literature:

In chlorobenzene; Schlenk technique; Reflux;

DOI:10.1021/ic500272b

Reference yield:

phosphorus(V) nitride + chlorine (7782-50-5) → 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine (940-71-6,16422-79-0) + cyclic polyphosphorus nitride dichloride + phosphorus pentachloride (10026-13-8,874483-75-7) + nitrogen (7727-37-9)

Guidance literature:

In neat (no solvent); formation of a mixt. of phosphorus nitride dichlorides with a large amount of (NPCl2)3 and a small amount of PCl5 by react. of P3N5 with Cl2 at 700 °C;;

Reference yield:

P4N6 + chlorine (7782-50-5) → 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine (940-71-6,16422-79-0) + cyclic polyphosphorus nitride dichloride + phosphorus pentachloride (10026-13-8,874483-75-7) + nitrogen (7727-37-9)

Guidance literature:

In neat (no solvent); formation of a mixt. of phosphorus nitride dichlorides with a large amount of (NPCl2)3 and a small amount of PCl5 by react. of P4N6 with Cl2 at 700 °C;;

upstream raw materials:

thionyl chloride

tetrasulfur tetranitride

phosphorus trichloride

mercury amidochloride

Downstream raw materials:

hexakis(4-formylphenoxy)cyclotriphosphazene

4-Methoxyphenyloxypentachlorcyclotriphosphazen