N-(3-phenyl-2-thioxo-2,5-dihydro-4,6-pyrimidinedionyl)-2-chlorobenzoic acid amide

Base Information

Chemical Name:N-(3-phenyl-2-thioxo-2,5-dihydro-4,6-pyrimidinedionyl)-2-chlorobenzoic acid amide
CAS No.:153260-29-8
Molecular Formula:C₁₇H₁₂ClN₃O₃S
Molecular Weight:373.82
Hs Code.:

Synonyms:N-(3-phenyl-2-thioxo-2,5-dihydro-4,6-pyrimidinedionyl)-2-chlorobenzoic acid amide

Suppliers and Price of N-(3-phenyl-2-thioxo-2,5-dihydro-4,6-pyrimidinedionyl)-2-chlorobenzoic acid amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(3-phenyl-2-thioxo-2,5-dihydro-4,6-pyrimidinedionyl)-2-chlorobenzoic acid amide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(3-phenyl-2-thioxo-2,5-dihydro-4,6-pyrimidinedionyl)-2-chlorobenzoic acid amide

There total 3 articles about N-(3-phenyl-2-thioxo-2,5-dihydro-4,6-pyrimidinedionyl)-2-chlorobenzoic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 141-82-2
malonic acid

: 26036-04-4
1-(o-chlorobenzoyl)-4-phenyl-3-thiosemicarbazide

: 153260-29-8
N-(3-phenyl-2-thioxo-2,5-dihydro-4,6-pyrimidinedionyl)-2-chlorobenzoic acid amide

Guidance literature:: With acetyl chloride; at 50 ℃; for 4h;
DOI:10.1016/0223-5234(93)90096-W

Reference yield:

: 103-72-0
phenyl isothiocyanate

: 153260-29-8
N-(3-phenyl-2-thioxo-2,5-dihydro-4,6-pyrimidinedionyl)-2-chlorobenzoic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 8 h / Heating

2: 70 percent / acetyl chloride / 4 h / 50 °C

With acetyl chloride; In ethanol;
DOI:10.1016/0223-5234(93)90096-W

Reference yield:

: 5814-05-1
2-chlorobenzoylhydrazide

: 153260-29-8
N-(3-phenyl-2-thioxo-2,5-dihydro-4,6-pyrimidinedionyl)-2-chlorobenzoic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 8 h / Heating

2: 70 percent / acetyl chloride / 4 h / 50 °C

With acetyl chloride; In ethanol;
DOI:10.1016/0223-5234(93)90096-W