[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] (2R)-2-nitromethyl-7-oxocycloheptanecarboxylate

Base Information

Chemical Name:[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] (2R)-2-nitromethyl-7-oxocycloheptanecarboxylate
CAS No.:1146352-92-2
Molecular Formula:C₂₅H₃₅NO₅
Molecular Weight:429.557
Hs Code.:

Synonyms:[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] (2R)-2-nitromethyl-7-oxocycloheptanecarboxylate

Suppliers and Price of [(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] (2R)-2-nitromethyl-7-oxocycloheptanecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] (2R)-2-nitromethyl-7-oxocycloheptanecarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] (2R)-2-nitromethyl-7-oxocycloheptanecarboxylate

There total 1 articles about [(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] (2R)-2-nitromethyl-7-oxocycloheptanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 75-52-5
nitromethane

: 1146352-87-5
[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] 7-oxocyclohept-1-enecarboxylate

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 1146352-92-2
[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] (2R)-2-nitromethyl-7-oxocycloheptanecarboxylate

: 1146352-89-7
[(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl] (7R,Z)-7-nitromethyl-2-(triisopropylsilyloxy)cyclohept-1-ene-1-carboxylate

Guidance literature:: nitromethane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.366667h; Inert atmosphere;

[(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl] 7-oxocyclohept-1-enecarboxylate; In tetrahydrofuran; hexane; at -78 ℃; for 1.83333h; Inert atmosphere;

triisopropylsilyl trifluoromethanesulfonate; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; hexane; at -78 - -10 ℃; Inert atmosphere;
DOI:10.1021/ol9003405