2-allyl-6-formyl-4-methoxycarbonyl-5-pivaloyloxymethylresorcinol dimethyl ether

Base Information

Chemical Name:2-allyl-6-formyl-4-methoxycarbonyl-5-pivaloyloxymethylresorcinol dimethyl ether
CAS No.:365972-50-5
Molecular Formula:C₂₀H₂₆O₇
Molecular Weight:378.422
Hs Code.:

Synonyms:2-allyl-6-formyl-4-methoxycarbonyl-5-pivaloyloxymethylresorcinol dimethyl ether

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Chemical Property of 2-allyl-6-formyl-4-methoxycarbonyl-5-pivaloyloxymethylresorcinol dimethyl ether

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Technology Process of 2-allyl-6-formyl-4-methoxycarbonyl-5-pivaloyloxymethylresorcinol dimethyl ether

There total 4 articles about 2-allyl-6-formyl-4-methoxycarbonyl-5-pivaloyloxymethylresorcinol dimethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 77-78-1
dimethyl sulfate

: 365972-49-2
2-allyl-6-formyl-4-methoxycarbonyl-5-pivaloyloxymethylresorcinol

: 365972-50-5
2-allyl-6-formyl-4-methoxycarbonyl-5-pivaloyloxymethylresorcinol dimethyl ether

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 6 ℃;
DOI:10.1081/SCC-100104047

Reference yield:

: 3282-30-2
pivaloyl chloride

: 365972-50-5
2-allyl-6-formyl-4-methoxycarbonyl-5-pivaloyloxymethylresorcinol dimethyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 56 percent / pyridine / CH₂Cl₂ / 20 °C

2: 32 percent / NaH / tetrahydrofuran / 2 h

3: 87 percent / NaH / dimethylformamide / 6 °C

With pyridine; sodium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1081/SCC-100104047

Reference yield:

: 365972-54-9
4-hydroxybut-2-yn-1-yl pivalate

: 365972-50-5
2-allyl-6-formyl-4-methoxycarbonyl-5-pivaloyloxymethylresorcinol dimethyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 32 percent / NaH / tetrahydrofuran / 2 h

2: 87 percent / NaH / dimethylformamide / 6 °C

With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1081/SCC-100104047