2-((5S,6S,E)-5-(dimethyl(phenyl)silyl)-6-hydroxy-7-methoxy-3-methylhept-3-en-1-yl)benzaldehyde

Base Information

Chemical Name:2-((5S,6S,E)-5-(dimethyl(phenyl)silyl)-6-hydroxy-7-methoxy-3-methylhept-3-en-1-yl)benzaldehyde
CAS No.:1404099-07-5
Molecular Formula:C₂₄H₃₂O₃Si
Molecular Weight:396.602
Hs Code.:

Synonyms:2-((5S,6S,E)-5-(dimethyl(phenyl)silyl)-6-hydroxy-7-methoxy-3-methylhept-3-en-1-yl)benzaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-((5S,6S,E)-5-(dimethyl(phenyl)silyl)-6-hydroxy-7-methoxy-3-methylhept-3-en-1-yl)benzaldehyde

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Technology Process of 2-((5S,6S,E)-5-(dimethyl(phenyl)silyl)-6-hydroxy-7-methoxy-3-methylhept-3-en-1-yl)benzaldehyde

There total 1 articles about 2-((5S,6S,E)-5-(dimethyl(phenyl)silyl)-6-hydroxy-7-methoxy-3-methylhept-3-en-1-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1404098-80-1
(2S,3S,E)-3-(dimethyl(phenyl)silyl)-7-(2-(hydroxymethyl)phenyl)-1-methoxy-5-methylhept-4-en-2-ol

: 1404099-07-5
2-((5S,6S,E)-5-(dimethyl(phenyl)silyl)-6-hydroxy-7-methoxy-3-methylhept-3-en-1-yl)benzaldehyde

Guidance literature:: With manganese(IV) oxide; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja3083945

Reference yield: 59.0%

: 1404099-07-5
2-((5S,6S,E)-5-(dimethyl(phenyl)silyl)-6-hydroxy-7-methoxy-3-methylhept-3-en-1-yl)benzaldehyde

: 1404099-15-5
(S)-1-((2S,3R,3aS,9bS)-3-(dimethyl(phenyl)silyl)-3a-methyl-2,3,3a,4,5,9b-hexahydronaphtho[1,2-b]furan-2-yl)-2-methoxyethanol

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -40 - -30 ℃; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ja3083945