N¹-Boc-N⁵-(1-imino-3-(N-tosyl)aminopropyl)-L-ornithine tert-butyl ester

Base Information

Chemical Name:N¹-Boc-N⁵-(1-imino-3-(N-tosyl)aminopropyl)-L-ornithine tert-butyl ester
CAS No.:884335-32-4
Molecular Formula:C₂₄H₄₀N₄O₆S
Molecular Weight:512.671
Hs Code.:

N<sup>1</sup>-Boc-N<sup>5</sup>-(1-imino-3-(N-tosyl)aminopropyl)-L-ornithine tert-butyl ester

Synonyms:N¹-Boc-N⁵-(1-imino-3-(N-tosyl)aminopropyl)-L-ornithine tert-butyl ester

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Chemical Property of N¹-Boc-N⁵-(1-imino-3-(N-tosyl)aminopropyl)-L-ornithine tert-butyl ester

Chemical Property:

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Technology Process of N¹-Boc-N⁵-(1-imino-3-(N-tosyl)aminopropyl)-L-ornithine tert-butyl ester

There total 5 articles about N¹-Boc-N⁵-(1-imino-3-(N-tosyl)aminopropyl)-L-ornithine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 96229-31-1
ethyl 3-(p-toluenesulfonylamino)-propionimidate hydrochloride

: 53054-03-8
tert-butyl (2S)-5-amino-2-[(2-methylpropan-2-yl)oxycarbonylamino]pentanoate

: 884335-32-4
N¹-Boc-N⁵-(1-imino-3-(N-tosyl)aminopropyl)-L-ornithine tert-butyl ester

Guidance literature:: In methanol; at 20 ℃; for 48h;
DOI:10.1016/j.bmc.2005.12.043

Reference yield:

: 2480-93-5
Boc-Orn(Z)-OH

: 884335-32-4
N¹-Boc-N⁵-(1-imino-3-(N-tosyl)aminopropyl)-L-ornithine tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / 4-(dimethylamino)pyridine / 2-methyl-propan-2-ol / 2 h

2: H₂ / Pd/C / methanol

3: 80 percent / methanol / 48 h / 20 °C

With dmap; hydrogen; palladium on activated charcoal; In methanol; tert-butyl alcohol;
DOI:10.1016/j.bmc.2005.12.043

Reference yield:

: 53054-02-7
N_α-(1,1-dimethylethoxycarbonyl)-N_δ-(phenylmethoxycarbonyl)-L-ornithine 1,1-dimethylethyl ester

: 884335-32-4
N¹-Boc-N⁵-(1-imino-3-(N-tosyl)aminopropyl)-L-ornithine tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol

2: 80 percent / methanol / 48 h / 20 °C

With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1016/j.bmc.2005.12.043