2-(1-(1-(phenylsulfonyl)-1H-indol-3-yl)propylidene)hydrazine-1-carboximidamide

Base Information

Chemical Name:2-(1-(1-(phenylsulfonyl)-1H-indol-3-yl)propylidene)hydrazine-1-carboximidamide
CAS No.:1262322-51-9
Molecular Formula:C₁₈H₁₉N₅O₂S
Molecular Weight:369.447
Hs Code.:

Synonyms:2-(1-(1-(phenylsulfonyl)-1H-indol-3-yl)propylidene)hydrazine-1-carboximidamide

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Chemical Property of 2-(1-(1-(phenylsulfonyl)-1H-indol-3-yl)propylidene)hydrazine-1-carboximidamide

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Technology Process of 2-(1-(1-(phenylsulfonyl)-1H-indol-3-yl)propylidene)hydrazine-1-carboximidamide

There total 4 articles about 2-(1-(1-(phenylsulfonyl)-1H-indol-3-yl)propylidene)hydrazine-1-carboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.3%

: 1937-19-5,16139-18-7
1-aminoguanidine hydrochloride

: 99532-49-7
1-[1-(benzenesulfonyl)-1H-indol-3-yl]propan-1-one

: 1262322-51-9
2-(1-(1-(phenylsulfonyl)-1H-indol-3-yl)propylidene)hydrazine-1-carboximidamide

Guidance literature:: 1-[1-(benzenesulfonyl)-1H-indol-3-yl]propan-1-one; With hydrogenchloride; In methanol; for 0.0833333h;

1-aminoguanidine hydrochloride; In methanol; at 110 ℃; for 2h;
DOI:10.1016/j.ejmech.2019.01.038

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 1262322-51-9
2-(1-(1-(phenylsulfonyl)-1H-indol-3-yl)propylidene)hydrazine-1-carboximidamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / dichloromethane / 20 °C

2.1: aluminum (III) chloride / dichloromethane / 0.33 h / 20 °C

2.2: 1 h

3.1: hydrogenchloride / methanol / 0.08 h

3.2: 2 h / 110 °C

With hydrogenchloride; aluminum (III) chloride; N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide; In methanol; dichloromethane;
DOI:10.1016/j.ejmech.2019.01.038

Reference yield:

: 40899-71-6
1-benzenesulfonylindole

: 1262322-51-9
2-(1-(1-(phenylsulfonyl)-1H-indol-3-yl)propylidene)hydrazine-1-carboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: aluminum (III) chloride / dichloromethane / 0.33 h / 20 °C

1.2: 1 h

2.1: hydrogenchloride / methanol / 0.08 h

2.2: 2 h / 110 °C

With hydrogenchloride; aluminum (III) chloride; In methanol; dichloromethane;
DOI:10.1016/j.ejmech.2019.01.038