1-(4-fluorophenyl)-2-(2-imino-1,3-oxazol-3(2H)-yl)ethanone hydrobromide

Base Information

Chemical Name:1-(4-fluorophenyl)-2-(2-imino-1,3-oxazol-3(2H)-yl)ethanone hydrobromide
CAS No.:815597-08-1
Molecular Formula:BrH*C₁₁H₉FN₂O₂
Molecular Weight:301.115
Hs Code.:

Synonyms:1-(4-fluorophenyl)-2-(2-imino-1,3-oxazol-3(2H)-yl)ethanone hydrobromide

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Chemical Property of 1-(4-fluorophenyl)-2-(2-imino-1,3-oxazol-3(2H)-yl)ethanone hydrobromide

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Technology Process of 1-(4-fluorophenyl)-2-(2-imino-1,3-oxazol-3(2H)-yl)ethanone hydrobromide

There total 1 articles about 1-(4-fluorophenyl)-2-(2-imino-1,3-oxazol-3(2H)-yl)ethanone hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 4570-45-0
2-amino-1,3-oxazole

: 403-29-2
2-bromo-4'-fluoroacetophenone

: 815597-08-1
1-(4-fluorophenyl)-2-(2-imino-1,3-oxazol-3(2H)-yl)ethanone hydrobromide

Guidance literature:: In tetrahydrofuran; acetonitrile; at 20 ℃; for 24.33h;

Reference yield: 92.0%

: 815597-08-1
1-(4-fluorophenyl)-2-(2-imino-1,3-oxazol-3(2H)-yl)ethanone hydrobromide

: 815597-09-2
6-(4-fluorophenyl)imidazo[2,1-b][1,3]oxazole

Guidance literature:: 1-(4-fluorophenyl)-2-(2-imino-1,3-oxazol-3(2H)-yl)ethanone hydrobromide; With titanium tetrachloride; In toluene; at -10 - 110 ℃; for 6.33h;

With sodium carbonate; In water; for 0.5h;

Reference yield:

: 815597-08-1
1-(4-fluorophenyl)-2-(2-imino-1,3-oxazol-3(2H)-yl)ethanone hydrobromide

: tert-butyl 4-({4-[6-(4-fluorophenyl)imidazo[2,1-b][1,3]oxazol-5-yl]pyrimidin-2-yl}amino)piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: titanium tetrachloride / toluene / 5.5 h / 0 °C / Heating / reflux

2: sulfuric acid / 1.5 h / 135 °C

3: 5 h / Heating / reflux

4: sodium ethanolate / ethanol / 15 h / Heating / reflux

With sulfuric acid; sodium ethanolate; titanium tetrachloride; In ethanol; toluene;