(1S,2S,5R)-(+)-neomenthyl phenyl sulfide

Base Information

Chemical Name:(1S,2S,5R)-(+)-neomenthyl phenyl sulfide
CAS No.:136944-69-9
Molecular Formula:C₁₆H₂₄S
Molecular Weight:248.433
Hs Code.:

Synonyms:(1S,2S,5R)-(+)-neomenthyl phenyl sulfide

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Chemical Property of (1S,2S,5R)-(+)-neomenthyl phenyl sulfide

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Technology Process of (1S,2S,5R)-(+)-neomenthyl phenyl sulfide

There total 3 articles about (1S,2S,5R)-(+)-neomenthyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 2230-82-2
menthyl tosylate

: 930-69-8
sodium thiophenolate

: 136944-69-9
(1S,2S,5R)-(+)-neomenthyl phenyl sulfide

Guidance literature:: sodium thiophenolate; With sodium hydride; In dimethyl sulfoxide; mineral oil; at 20 ℃; for 0.5h; Inert atmosphere;

menthyl tosylate; In dimethyl sulfoxide; mineral oil; at 90 ℃; for 10h; Inert atmosphere;
DOI:10.1080/10426507.2013.819867

Reference yield: 52.0%

: 2230-82-2
menthyl tosylate

: 108-98-5
thiophenol

: 136944-69-9
(1S,2S,5R)-(+)-neomenthyl phenyl sulfide

Guidance literature:: thiophenol; With potassium hydroxide; In ethanol; at 60 ℃;

menthyl tosylate; In ethanol; at 78 ℃;
DOI:10.1002/chir.22454

Reference yield:

: 2216-51-5
(-)-menthol

: 136944-69-9
(1S,2S,5R)-(+)-neomenthyl phenyl sulfide

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 0 °C

2.1: potassium hydroxide / ethanol / 60 °C

2.2: 78 °C

With pyridine; potassium hydroxide; In ethanol;
DOI:10.1002/chir.22454