2-(9H-Carbazol-9-yl)ethyl methacrylate

Base Information

• Chemical Name: 2-(9H-Carbazol-9-yl)ethyl methacrylate
• CAS No.: 15657-91-7
• Molecular Formula: C18H17NO2
• Molecular Weight: 279.33308
• Hs Code.: 2933990090
• European Community (EC) Number: 683-370-1
• DSSTox Substance ID: DTXSID70364924
• Nikkaji Number: J662.866D
• Wikidata: Q82149154
• Mol file: 15657-91-7.mol

Synonyms:2-(9H-Carbazol-9-yl)ethyl methacrylate;15657-91-7;9H-Carbazole-9-ethylmethacrylate;2-carbazol-9-ylethyl 2-methylprop-2-enoate;2-Propenoic acid, 2-methyl-, 2-(9H-carbazol-9-yl)ethyl ester;2-(9H-carbazol-9-yl)ethyl 2-methylprop-2-enoate;SCHEMBL957686;DTXSID70364924;9H-Carbazole-9-ethanol methacrylate;MFCD00085236;STK367283;AKOS005443869;2-(9H-Carbazol-9-yl)ethylmethacrylate;BS-15496;2-(9h-carbazole-9-yl) ethyl methacrylate;CS-0318487;FT-0743522;D83707;J-009316

Chemical Property of 2-(9H-Carbazol-9-yl)ethyl methacrylate

Chemical Property:

• Vapor Pressure: 1.63E-06mmHg at 25°C
• Melting Point: 72.7-79.4 °C(lit.)
• Refractive Index: 1.585
• Boiling Point: 397.1°C at 760 mmHg
• Flash Point: 194°C
• PSA: 31.23000
• Density: 1.11g/cm³
• LogP: 3.91380
• Storage Temp.: 2-8°C
• XLogP3: 4.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 279.125928785
• Heavy Atom Count: 21
• Complexity: 384

Purity/Quality:

98%,99%, ^*data from raw suppliers

9H-Carbazole-9-ethylmethacrylate ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-28

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=C)C(=O)OCCN1C2=CC=CC=C2C3=CC=CC=C31

Technology Process of 2-(9H-Carbazol-9-yl)ethyl methacrylate

There total 8 articles about 2-(9H-Carbazol-9-yl)ethyl methacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2-carbazol-9-yl-ethanol (1484-14-6) + Methacryloyl chloride (920-46-7,26937-45-1) → N-(2-hydroxyethyl)carbazolyl methacrylate (15657-91-7)

Guidance literature:

With triethylamine; hydroquinone; In dichloromethane; at 0 - 5 ℃; for 48h;

DOI:10.1039/b102489m

Reference yield: 85.0%

2-carbazol-9-yl-ethanol (1484-14-6) + poly(methacrylic acid) (79-41-4,25087-26-7,50867-57-7) → N-(2-hydroxyethyl)carbazolyl methacrylate (15657-91-7)

Guidance literature:

With 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In 1,2-dichloro-ethane; at 20 ℃; for 24h;

DOI:10.1080/15421400801904732

Reference yield: 61.0%

2-carbazol-9-yl-ethanol (1484-14-6) + methacryloyl anhydride (760-93-0) → N-(2-hydroxyethyl)carbazolyl methacrylate (15657-91-7)

Guidance literature:

With pyridine; dmap; 4-methoxy-phenol; for 0.166667h; Heating;

upstream raw materials:

2-carbazol-9-yl-ethanol

Methacryloyl chloride

methacryloyl anhydride

poly(methacrylic acid)