1-(1,1-dimethylethyl) 3-ethyl 2',3'-dimethyl-6'-[(phenylmethyl)oxy]-5,6-dihydro-4,4'-bipyridine-1,3(2H)-dicarboxylate

Base Information

Chemical Name:1-(1,1-dimethylethyl) 3-ethyl 2',3'-dimethyl-6'-[(phenylmethyl)oxy]-5,6-dihydro-4,4'-bipyridine-1,3(2H)-dicarboxylate
CAS No.:1194489-45-6
Molecular Formula:C₂₇H₃₄N₂O₅
Molecular Weight:466.577
Hs Code.:

Synonyms:1-(1,1-dimethylethyl) 3-ethyl 2',3'-dimethyl-6'-[(phenylmethyl)oxy]-5,6-dihydro-4,4'-bipyridine-1,3(2H)-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(1,1-dimethylethyl) 3-ethyl 2',3'-dimethyl-6'-[(phenylmethyl)oxy]-5,6-dihydro-4,4'-bipyridine-1,3(2H)-dicarboxylate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1-(1,1-dimethylethyl) 3-ethyl 2',3'-dimethyl-6'-[(phenylmethyl)oxy]-5,6-dihydro-4,4'-bipyridine-1,3(2H)-dicarboxylate

There total 4 articles about 1-(1,1-dimethylethyl) 3-ethyl 2',3'-dimethyl-6'-[(phenylmethyl)oxy]-5,6-dihydro-4,4'-bipyridine-1,3(2H)-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1194488-90-8
4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-5,6-dihydro-2H-pyridine-1,3-dicarboxylic acid 1-tert-butyl ester 3-ethyl ester

: 1194493-06-5
4-bromo-2,3-dimethyl-6-[(phenylmethyl)oxy]pyridine

: 1194489-45-6
1-(1,1-dimethylethyl) 3-ethyl 2',3'-dimethyl-6'-[(phenylmethyl)oxy]-5,6-dihydro-4,4'-bipyridine-1,3(2H)-dicarboxylate

Guidance literature:: With sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In propan-1-ol; water; at 80 ℃; for 18h; Inert atmosphere;

Reference yield:

: 100-39-0
benzyl bromide

: 1194489-45-6
1-(1,1-dimethylethyl) 3-ethyl 2',3'-dimethyl-6'-[(phenylmethyl)oxy]-5,6-dihydro-4,4'-bipyridine-1,3(2H)-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: silver carbonate / benzene / 72 h / 45 °C / in the dark; Inert atmosphere

2: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / propan-1-ol; water / 18 h / 80 °C / Inert atmosphere

With sodium carbonate; silver carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In propan-1-ol; water; benzene;

Reference yield:

: 176525-98-7
1-(1,1-dimethylethyl) 3-ethyl 4-{[(trifluoromethyl)sulfonyl]oxy}-1,2,5,6-tetrahydropyridine-1,3-dicarboxylate

: 1194489-45-6
1-(1,1-dimethylethyl) 3-ethyl 2',3'-dimethyl-6'-[(phenylmethyl)oxy]-5,6-dihydro-4,4'-bipyridine-1,3(2H)-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 14 h / 80 °C / Inert atmosphere

2: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / propan-1-ol; water / 18 h / 80 °C / Inert atmosphere

With potassium acetate; sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; propan-1-ol; water;