2-[5-(4-methoxy-benzyl)-[1,3,4]oxadiazol-2-ylsulfanyl]-1-phenyl-ethanone

Base Information

• Chemical Name: 2-[5-(4-methoxy-benzyl)-[1,3,4]oxadiazol-2-ylsulfanyl]-1-phenyl-ethanone
• CAS No.: 302949-15-1
• Molecular Formula: C₁₈H₁₆N₂O₃S
• Molecular Weight: 340.403

Synonyms:2-[5-(4-methoxy-benzyl)-[1,3,4]oxadiazol-2-ylsulfanyl]-1-phenyl-ethanone

Chemical Property of 2-[5-(4-methoxy-benzyl)-[1,3,4]oxadiazol-2-ylsulfanyl]-1-phenyl-ethanone

Chemical Property:

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Technology Process of 2-[5-(4-methoxy-benzyl)-[1,3,4]oxadiazol-2-ylsulfanyl]-1-phenyl-ethanone

There total 2 articles about 2-[5-(4-methoxy-benzyl)-[1,3,4]oxadiazol-2-ylsulfanyl]-1-phenyl-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

α-bromoacetophenone (70-11-1) + 5-(4-methoxybenzyl)-1,3,4-oxadiazole-2(3H)-thione (93073-37-1) → 2-[5-(4-methoxy-benzyl)-[1,3,4]oxadiazol-2-ylsulfanyl]-1-phenyl-ethanone (302949-15-1)

Guidance literature:

With potassium hydroxide; In ethanol; water; at 20 ℃;

DOI:10.1023/A:1013946509227

Reference yield:

2-(4-methoxyphenyl)acetic acid hydrazide (57676-49-0) → 2-[5-(4-methoxy-benzyl)-[1,3,4]oxadiazol-2-ylsulfanyl]-1-phenyl-ethanone (302949-15-1)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH / Heating

2: 68 percent / KOH / ethanol; H₂O / 20 °C

With potassium hydroxide; In ethanol; water;

DOI:10.1023/A:1013946509227

Reference yield: 76.0%

2-[5-(4-methoxy-benzyl)-[1,3,4]oxadiazol-2-ylsulfanyl]-1-phenyl-ethanone (302949-15-1) → 2-(4-methoxy-phenyl)-N-(2-oxo-4-phenyl-thiazol-3-yl)-acetamide

Guidance literature:

With hydrogenchloride; In ethanol; for 1h; Heating;

DOI:10.1023/A:1013946509227

upstream raw materials:

α-bromoacetophenone

5-(4-methoxybenzyl)-1,3,4-oxadiazole-2(3H)-thione

2-(4-methoxyphenyl)acetic acid hydrazide

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