Methyl α-azido-2-<(2E,4E)-4-phenylbuta-1,3-dienyl>-4,5-dimethoxycinnamate

Base Information

Chemical Name:Methyl α-azido-2-<(2E,4E)-4-phenylbuta-1,3-dienyl>-4,5-dimethoxycinnamate
CAS No.:171895-16-2
Molecular Formula:C₂₂H₂₁N₃O₄
Molecular Weight:391.426
Hs Code.:

Synonyms:Methyl α-azido-2-<(2E,4E)-4-phenylbuta-1,3-dienyl>-4,5-dimethoxycinnamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl α-azido-2-<(2E,4E)-4-phenylbuta-1,3-dienyl>-4,5-dimethoxycinnamate

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Technology Process of Methyl α-azido-2-<(2E,4E)-4-phenylbuta-1,3-dienyl>-4,5-dimethoxycinnamate

There total 4 articles about Methyl α-azido-2-<(2E,4E)-4-phenylbuta-1,3-dienyl>-4,5-dimethoxycinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1816-92-8
Methyl azidoacetate

: 171733-10-1
4,5-Dimethoxy-2-((1E,3E)-4-phenyl-buta-1,3-dienyl)-benzaldehyde

: 171895-16-2
Methyl α-azido-2-<(2E,4E)-4-phenylbuta-1,3-dienyl>-4,5-dimethoxycinnamate

Guidance literature:: With sodium methylate; In tetrahydrofuran; methanol; dichloromethane; for 3h; Ambient temperature;

Reference yield:

: 5392-10-9
2-bromo-4,5-dimethoxybenzaldehyde

: 171895-16-2
Methyl α-azido-2-<(2E,4E)-4-phenylbuta-1,3-dienyl>-4,5-dimethoxycinnamate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) n-BuLi / 2) THF, r.t.

3: NaOMe / methanol

With n-butyllithium; sodium methylate; In methanol;
DOI:10.1016/0040-4039(91)80343-5

Reference yield:

: 38633-40-8
(E)-cinnamyltriphenylphosphonium bromide

: 171895-16-2
Methyl α-azido-2-<(2E,4E)-4-phenylbuta-1,3-dienyl>-4,5-dimethoxycinnamate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) n-BuLi / 2) THF, r.t.

3: NaOMe / methanol

With n-butyllithium; sodium methylate; In methanol;
DOI:10.1016/0040-4039(91)80343-5