((C₂H₅)8C₂₀H₄N₄)Rh(CH₂CH₂C₆H₅)

Base Information

Chemical Name:((C₂H₅)8C₂₀H₄N₄)Rh(CH₂CH₂C₆H₅)
CAS No.:96502-53-3
Molecular Formula:C₄₄H₅₃N₄Rh
Molecular Weight:740.837
Hs Code.:

((C<sub>2</sub>H<sub>5</sub>)8C<sub>20</sub>H<sub>4</sub>N<sub>4</sub>)Rh(CH<sub>2</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)

Synonyms:((C₂H₅)8C₂₀H₄N₄)Rh(CH₂CH₂C₆H₅)

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Chemical Property of ((C₂H₅)8C₂₀H₄N₄)Rh(CH₂CH₂C₆H₅)

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Technology Process of ((C₂H₅)8C₂₀H₄N₄)Rh(CH₂CH₂C₆H₅)

There total 4 articles about ((C₂H₅)8C₂₀H₄N₄)Rh(CH₂CH₂C₆H₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 63439-10-1
octaethylporphyrinatorhodium(II) dimer

: 100-41-4,27536-89-6
ethylbenzene

: 63372-77-0
(octaethylporphyrinato)(hydrido)rhodium(II)

: 96502-53-3
((C₂H₅)8C₂₀H₄N₄)Rh(CH₂CH₂C₆H₅)

: 99248-50-7
((C₂H₅)8C₂₀H₄N₄)Rh(CH(C₆H₅)CH₃)

Guidance literature:: In not given; Schlenk techniques, thermal react. of Rh-complex with ethylbenzene in sealed tube in the dark for 24 h at 109°C;
DOI:10.1021/ja00312a023

Reference yield: 45.0%

: 63372-77-0
(octaethylporphyrinato)(hydrido)rhodium(II)

: 103-63-9
1-phenyl-2-bromoethane

: 96502-53-3
((C₂H₅)8C₂₀H₄N₄)Rh(CH₂CH₂C₆H₅)

Guidance literature:: With hydroxide; In methanol; benzene; Rh-complex anion was generated by adding 0.5 N OH(1-)/MeOH to Rh-complex in C6H6 under Ar, stirred for 15 min, slight excess of PhCH2CH2Br added, stirred for 10 min; evapd. in vac., chromd. (SiO2, C6H6), dried in vac.;
DOI:10.1021/ja00312a023

Reference yield: 20.0%

: 63439-10-1
octaethylporphyrinatorhodium(II) dimer

: 100-41-4,27536-89-6
ethylbenzene

: 96502-53-3
((C₂H₅)8C₂₀H₄N₄)Rh(CH₂CH₂C₆H₅)

Guidance literature:: In not given; Schlenk techniques, thermal react. of Rh-complex with ethylbenzene in sealed tube in the dark for 3 h at 160°C;
DOI:10.1021/ja00312a023