tert-butoxycarbonylamino-{3-[3-(2-methoxy-phenyl)-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridin-5-yl]-phenyl}-acetic acid

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Chemical Name:tert-butoxycarbonylamino-{3-[3-(2-methoxy-phenyl)-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridin-5-yl]-phenyl}-acetic acid
CAS No.:1071454-33-5
Molecular Formula:C₃₄H₃₃N₃O₇S
Molecular Weight:627.718
Hs Code.:

Synonyms:tert-butoxycarbonylamino-{3-[3-(2-methoxy-phenyl)-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridin-5-yl]-phenyl}-acetic acid

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Chemical Property of tert-butoxycarbonylamino-{3-[3-(2-methoxy-phenyl)-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridin-5-yl]-phenyl}-acetic acid

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Technology Process of tert-butoxycarbonylamino-{3-[3-(2-methoxy-phenyl)-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridin-5-yl]-phenyl}-acetic acid

There total 1 articles about tert-butoxycarbonylamino-{3-[3-(2-methoxy-phenyl)-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridin-5-yl]-phenyl}-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 82278-95-3
rac-(3-(3-bromophenyl)-2-tert-butoxycarbonylamino)propionic acid

: 875639-17-1
3-(2-methoxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-tosyl-1H-pyrrolo[2,3-b]pyridine

: 1071454-33-5
tert-butoxycarbonylamino-{3-[3-(2-methoxy-phenyl)-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridin-5-yl]-phenyl}-acetic acid

Guidance literature:: rac-(3-(3-bromophenyl)-2-tert-butoxycarbonylamino)propionic acid; 3-(2-methoxyphenyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-tosyl-1H-pyrrolo[2,3-b]pyridine; With sodium carbonate; In tetrahydrofuran; water; acetonitrile; for 0.0166667h;

(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; water; acetonitrile; at 120 ℃; for 0.35h; Microwave irradiation;

Reference yield: 35.0%

: 1071454-33-5
tert-butoxycarbonylamino-{3-[3-(2-methoxy-phenyl)-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridin-5-yl]-phenyl}-acetic acid

: 124-40-3
dimethyl amine

: 1071451-73-4
2-amino-2-{3-[3-(2-methoxy-phenyl)-1H-pyrrolo[2,3-b]pyridin-5-yl]-phenyl}-N,N-dimethyl-acetamide

Guidance literature:: tert-butoxycarbonylamino-{3-[3-(2-methoxy-phenyl)-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridin-5-yl]-phenyl}-acetic acid; dimethyl amine; With N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 1h;

With potassium hydroxide; water; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; for 0.5h;

With trifluoroacetic acid;