ALLYL-(2-METHOXY-PHENYL)-AMINE

Base Information

• Chemical Name: ALLYL-(2-METHOXY-PHENYL)-AMINE
• CAS No.: 15258-47-6
• Molecular Formula: C10H13 N O
• Molecular Weight: 163.219
• Hs Code.: 2922299090
• Mol file: 15258-47-6.mol

Synonyms:Benzenamine,2-methoxy-N-2-propenyl- (9CI); o-Anisidine, N-allyl- (8CI);N-Allyl-2-methoxyaniline; N-Allyl-o-anisidine

Chemical Property of ALLYL-(2-METHOXY-PHENYL)-AMINE

Chemical Property:

• Vapor Pressure: 0.0294mmHg at 25°C
• Refractive Index: 1.553
• Boiling Point: 245°C at 760 mmHg
• PKA: 4.06±0.50(Predicted)
• Flash Point: 96°C
• PSA: 21.26000
• Density: 1.013g/cm³
• LogP: 2.36610

Purity/Quality:

99% ^*data from raw suppliers

ALLYL-(2-METHOXY-PHENYL)-AMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ALLYL-(2-METHOXY-PHENYL)-AMINE

There total 11 articles about ALLYL-(2-METHOXY-PHENYL)-AMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-bromoanisole (578-57-4) + 1-amino-2-propene (107-11-9,30551-89-4) → 2-methoxy-N-allylaniline (15258-47-6)

Guidance literature:

With potassium phosphate; copper(l) iodide; L-proline; In dimethyl sulfoxide; at 90 ℃; for 40h;

DOI:10.1021/jo0504464

Reference yield: 89.0%

2-methoxy-phenylamine (90-04-0) + allyl bromide (106-95-6) → 2-methoxy-N-allylaniline (15258-47-6)

Guidance literature:

In water; acetonitrile; at 70 ℃; for 0.166667h; Microwave irradiation;

DOI:10.1016/j.tetlet.2014.03.044

Reference yield: 84.0%

2-methoxy-phenylamine (90-04-0) + allyl alcohol (107-18-6) → 2-methoxy-N-allylaniline (15258-47-6)

Guidance literature:

With 1,1'-bis-(diphenylphosphino)ferrocene; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; tetrabutylammonium acetate; In acetonitrile; at 60 ℃; for 18h; chemoselective reaction; Inert atmosphere; Schlenk technique; Glovebox; Molecular sieve;

DOI:10.1002/chem.201502329

upstream raw materials:

2-methoxy-phenylamine

allyl bromide

2-bromoanisole

1-amino-2-propene

Downstream raw materials:

benzoxazole

1,2-benzisoxazole

o-aminobenzaldehyde

aniline

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