1-(4-dodecyloxy-5-methoxy-2-nitrobenzyloxy)-2,4-bis(3,5-diformylphenoxy)benzene

Base Information

Chemical Name:1-(4-dodecyloxy-5-methoxy-2-nitrobenzyloxy)-2,4-bis(3,5-diformylphenoxy)benzene
CAS No.:760984-02-9
Molecular Formula:C₄₄H₄₉NO₁₁
Molecular Weight:767.873
Hs Code.:

Synonyms:1-(4-dodecyloxy-5-methoxy-2-nitrobenzyloxy)-2,4-bis(3,5-diformylphenoxy)benzene

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Chemical Property of 1-(4-dodecyloxy-5-methoxy-2-nitrobenzyloxy)-2,4-bis(3,5-diformylphenoxy)benzene

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Technology Process of 1-(4-dodecyloxy-5-methoxy-2-nitrobenzyloxy)-2,4-bis(3,5-diformylphenoxy)benzene

There total 3 articles about 1-(4-dodecyloxy-5-methoxy-2-nitrobenzyloxy)-2,4-bis(3,5-diformylphenoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 3328-70-9
5-formyl-2-hydroxybenzaldehyde

: 760983-94-6
1-(4-dodecyloxy-5-methoxy-2-nitrobenzyloxy)-2,4-bis(chloromethyl)benzene

: 760984-02-9
1-(4-dodecyloxy-5-methoxy-2-nitrobenzyloxy)-2,4-bis(3,5-diformylphenoxy)benzene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 48h;
DOI:10.1016/j.tet.2004.06.078

Reference yield:

: 3328-70-9
5-formyl-2-hydroxybenzaldehyde

: 760984-02-9
1-(4-dodecyloxy-5-methoxy-2-nitrobenzyloxy)-2,4-bis(3,5-diformylphenoxy)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / K₂CO₃ / dimethylformamide / 40 °C

2: 93 percent / NaBH₄ / tetrahydrofuran; methanol / 1 h / 20 °C

3: 95 percent / SOCl₂ / CH₂Cl₂ / 0.33 h / 20 °C

4: 52 percent / K₂CO₃ / dimethylformamide / 48 h / 50 °C

With sodium tetrahydroborate; thionyl chloride; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2004.06.078

Reference yield:

: 4-dodecyloxy-5-methoxy-2-nitrobenzyl bromide

: 760984-02-9
1-(4-dodecyloxy-5-methoxy-2-nitrobenzyloxy)-2,4-bis(3,5-diformylphenoxy)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / K₂CO₃ / dimethylformamide / 40 °C

2: 93 percent / NaBH₄ / tetrahydrofuran; methanol / 1 h / 20 °C

3: 95 percent / SOCl₂ / CH₂Cl₂ / 0.33 h / 20 °C

4: 52 percent / K₂CO₃ / dimethylformamide / 48 h / 50 °C

With sodium tetrahydroborate; thionyl chloride; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2004.06.078