C₂₆H₂₂FNO₇S

Base Information

Chemical Name:C₂₆H₂₂FNO₇S
CAS No.:1374233-80-3
Molecular Formula:C₂₆H₂₂FNO₇S
Molecular Weight:511.528
Hs Code.:

C<sub>26</sub>H<sub>22</sub>FNO<sub>7</sub>S

Synonyms:C₂₆H₂₂FNO₇S

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Chemical Property of C₂₆H₂₂FNO₇S

Chemical Property:

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Technology Process of C₂₆H₂₂FNO₇S

There total 11 articles about C₂₆H₂₂FNO₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374233-79-0
C₂₅H₂₀FNO₅

: 124-63-0
methanesulfonyl chloride

: 1374233-80-3
C₂₆H₂₂FNO₇S

Guidance literature:: With pyridine; at 0 - 30 ℃; for 2h;

Reference yield:

: 99-90-1
para-bromoacetophenone

: 1374233-80-3
C₂₆H₂₂FNO₇S

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydride / toluene; mineral oil / 2 h / 0 - 20 °C

1.2: Reflux

2.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

3.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

3.2: 4 h / 80 °C

4.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

5.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

6.1: boron trichloride / dichloromethane / -78 - -40 °C

7.1: triethylamine / dmap / dichloromethane / 1 h / 0 - 20 °C

8.1: sodium acetate / (diphenylphosphin)ferrocene; palladium diacetate / acetonitrile / 2 h / 100 °C / Inert atmosphere

9.1: hydrogenchloride; water / tetrahydrofuran / 1 h / Reflux

10.1: tin(II) chloride dihdyrate / ethyl acetate / 1 h / 80 °C

10.2: 20 °C / pH 8 - 9

11.1: pyridine / 2 h / 0 - 30 °C

With pyridine; hydrogenchloride; potassium phosphate; tin(II) chloride dihdyrate; water; nitric acid; sodium acetate; boron trichloride; sodium hydride; caesium carbonate; triethylamine; zinc(II) chloride; dmap; (diphenylphosphin)ferrocene; palladium diacetate; tert-butyl XPhos; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil;

Reference yield:

: 26510-95-2
ethyl 4-Bromobenzoylacetate

: 1374233-80-3
C₂₆H₂₂FNO₇S

Guidance literature:: Multi-step reaction with 10 steps

1.1: zinc(II) chloride / N,N-dimethyl-formamide / 3.5 h / 105 °C

2.1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 0.33 h / 20 °C

2.2: 4 h / 80 °C

3.1: nitric acid / dichloromethane / 1.5 h / 0 - 20 °C

4.1: potassium phosphate / palladium diacetate; tert-butyl XPhos / toluene / 2 h / 100 °C / Inert atmosphere

5.1: boron trichloride / dichloromethane / -78 - -40 °C

6.1: triethylamine / dmap / dichloromethane / 1 h / 0 - 20 °C

7.1: sodium acetate / (diphenylphosphin)ferrocene; palladium diacetate / acetonitrile / 2 h / 100 °C / Inert atmosphere

8.1: hydrogenchloride; water / tetrahydrofuran / 1 h / Reflux

9.1: tin(II) chloride dihdyrate / ethyl acetate / 1 h / 80 °C

9.2: 20 °C / pH 8 - 9

10.1: pyridine / 2 h / 0 - 30 °C

With pyridine; hydrogenchloride; potassium phosphate; tin(II) chloride dihdyrate; water; nitric acid; sodium acetate; boron trichloride; caesium carbonate; triethylamine; zinc(II) chloride; dmap; (diphenylphosphin)ferrocene; palladium diacetate; tert-butyl XPhos; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile;