BENZYL-ALPHA,ALPHA-D2-AMINE

Base Information

• Chemical Name: BENZYL-ALPHA,ALPHA-D2-AMINE
• CAS No.: 15185-02-1
• Molecular Formula: C7H7 D2 N
• Molecular Weight: 109.139
• Mol file: 15185-02-1.mol

Synonyms:Benzyl-a,a-d2-amine (8CI); a,a-Dideuteriobenzylamine; a-Dideuteriobenzylamine

Chemical Property of BENZYL-ALPHA,ALPHA-D2-AMINE

Chemical Property:

• Boiling Point: 63-65 °C(Press: 20 Torr)
• PSA: 26.02000
• LogP: 1.84560

Purity/Quality:

BENZYL-ALPHA-ALPHA-D2-AMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Benzyl-alpha,alpha-d2-amine (CAS# 15185-02-1) is a useful isotopically labeled research compound.

Technology Process of BENZYL-ALPHA,ALPHA-D2-AMINE

There total 7 articles about BENZYL-ALPHA,ALPHA-D2-AMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

benzonitrile (100-47-0) → 1,1-dideuteriobenzylamine (15185-02-1)

Guidance literature:

With lithium aluminium deuteride; In diethyl ether; at 25 ℃; for 4.5h;

DOI:10.1021/jo00016a026

Reference yield:

benzamide (55-21-0,27208-38-4) → 1,1-dideuteriobenzylamine (15185-02-1)

Guidance literature:

With lithium aluminium deuteride; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere; Reflux;

DOI:10.1021/ol500670h

Reference yield:

<α-D2>Benzylazid → 1,1-dideuteriobenzylamine (15185-02-1)

Guidance literature:

With water; triphenylphosphine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1002/chem.201503823

upstream raw materials:

benzonitrile

benzamide

[1',1'-2H₂]benzyl bromide

benzoic acid ethyl ester

Downstream raw materials:

<1-2H2>benzyl-p-nitrophenyltriazene

N-(2,2-dichloro-1-phenylcyclopropylmethylene)-α,α-dideuteriobenzylamine

1,1-dideuteriophenylmethanol

benzyl-d2 chloride

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