(3S,4S)-4-methyl-4-phenyl-3-tris(trimethylsilyl)siloxybutanal

Base Information

Chemical Name:(3S,4S)-4-methyl-4-phenyl-3-tris(trimethylsilyl)siloxybutanal
CAS No.:875288-47-4
Molecular Formula:C₂₀H₄₀O₂Si₄
Molecular Weight:424.878
Hs Code.:

Synonyms:(3S,4S)-4-methyl-4-phenyl-3-tris(trimethylsilyl)siloxybutanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S)-4-methyl-4-phenyl-3-tris(trimethylsilyl)siloxybutanal

Chemical Property:

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Technology Process of (3S,4S)-4-methyl-4-phenyl-3-tris(trimethylsilyl)siloxybutanal

There total 4 articles about (3S,4S)-4-methyl-4-phenyl-3-tris(trimethylsilyl)siloxybutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 861445-91-2
tris(trimethylsilyl)-vinyloxy-silane

: 93-53-8
(S)-2-phenyl-propionaldehyde

: 875288-47-4
(3S,4S)-4-methyl-4-phenyl-3-tris(trimethylsilyl)siloxybutanal

Guidance literature:: With bis(trifluoromethanesulfonyl)amide; In dichloromethane; at -78 ℃; for 0.5h;
DOI:10.1021/ja0693542

Reference yield:

: 861445-91-2
tris(trimethylsilyl)-vinyloxy-silane

: 93-53-8
(S)-2-phenyl-propionaldehyde

: (3R,4S)-4-methyl-4-phenyl-3-tris(trimethylsilyl)siloxybutanal

: 875288-47-4
(3S,4S)-4-methyl-4-phenyl-3-tris(trimethylsilyl)siloxybutanal

Guidance literature:: With bis(trifluoromethanesulfonyl)amide; In dichloromethane; at -78 - 20 ℃; for 0.25h; Title compound not separated from byproducts;
DOI:10.1021/ja054725k

Reference yield:

: 37778-99-7
(S)-2-phenyl-1-propanol

: 875288-47-4
(3S,4S)-4-methyl-4-phenyl-3-tris(trimethylsilyl)siloxybutanal

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodane

2: HNTf₂ / CH₂Cl₂ / 0.5 h / -78 °C

With Dess-Martin periodane; bis(trifluoromethanesulfonyl)amide; In dichloromethane;
DOI:10.1021/ja0693542