ethyl 2-diazo-3-[4-(3,5-dichloropyrid-4-ylcarboxamido)phenyl]propionate

Base Information

• Chemical Name: ethyl 2-diazo-3-[4-(3,5-dichloropyrid-4-ylcarboxamido)phenyl]propionate
• CAS No.: 263276-16-0
• Molecular Formula: C₁₇H₁₄Cl₂N₄O₃
• Molecular Weight: 393.229

Synonyms:ethyl 2-diazo-3-[4-(3,5-dichloropyrid-4-ylcarboxamido)phenyl]propionate

Chemical Property of ethyl 2-diazo-3-[4-(3,5-dichloropyrid-4-ylcarboxamido)phenyl]propionate

Chemical Property:

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Technology Process of ethyl 2-diazo-3-[4-(3,5-dichloropyrid-4-ylcarboxamido)phenyl]propionate

There total 1 articles about ethyl 2-diazo-3-[4-(3,5-dichloropyrid-4-ylcarboxamido)phenyl]propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N-isonicotinoyl-(L)-4-aminophenylalanine (263276-28-4) → ethyl 2-diazo-3-[4-(3,5-dichloropyrid-4-ylcarboxamido)phenyl]propionate (263276-16-0)

Guidance literature:

With acetic acid; isopentyl nitrite; In chloroform; for 1h; Heating / reflux;

Reference yield:

2-amino-4-thio-n-propylpyridine + ethyl 2-diazo-3-[4-(3,5-dichloropyrid-4-ylcarboxamido)phenyl]propionate (263276-16-0) → ethyl 3-[4-(3,5-dichloropyrid-4-ylcarboxamido)phenyl]-2-(4-propylthiopyridine-2-amino)propionate (263275-29-2)

Guidance literature:

With dirhodium tetraacetate; In toluene; at 80 ℃;

DOI:10.1016/S0960-894X(02)00241-X

Reference yield:

5-chloro-2-pyridylamine (1072-98-6) + ethyl 2-diazo-3-[4-(3,5-dichloropyrid-4-ylcarboxamido)phenyl]propionate (263276-16-0) → ethyl 3-[4-(3,5-dichloropyrid-4-ylcarboxamido)phenyl]-2-(5-chloropyridine-2-amino)propionate (263275-28-1)

Guidance literature:

With dirhodium tetraacetate; In toluene; Heating;

DOI:10.1016/S0960-894X(02)00241-X

upstream raw materials:

N-isonicotinoyl-(L)-4-aminophenylalanine

Downstream raw materials:

ethyl 3-[4-(3,5-dichloropyrid-4-ylcarboxamido)phenyl]-2-(5-chloropyridine-2-amino)propionate

ethyl 3-[4-(3,5-dichloropyrid-4-ylcarboxamido)phenyl]-2-(4-propylthiopyridine-2-amino)propionate

ethyl 3-[4-(3,5-dichloropyrid-4-ylcarboxamido)phenyl]-2-(5-chloro-4-propylthiopyridine-2-amino)propionate

ethyl 3-[4-(3,5-dichloropyrid-4-ylcarboxamido)phenyl]-2-(5-chloro-4-propylsulphinylpyridine-2-amino)propionate

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