tert-butyl ((1-(4-aminophenyl)cyclopropyl)methyl)(cyclopropyl)carbamate

Base Information

Chemical Name:tert-butyl ((1-(4-aminophenyl)cyclopropyl)methyl)(cyclopropyl)carbamate
CAS No.:1308815-49-7
Molecular Formula:C₁₈H₂₆N₂O₂
Molecular Weight:302.417
Hs Code.:

Synonyms:tert-butyl ((1-(4-aminophenyl)cyclopropyl)methyl)(cyclopropyl)carbamate

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Chemical Property of tert-butyl ((1-(4-aminophenyl)cyclopropyl)methyl)(cyclopropyl)carbamate

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Technology Process of tert-butyl ((1-(4-aminophenyl)cyclopropyl)methyl)(cyclopropyl)carbamate

There total 5 articles about tert-butyl ((1-(4-aminophenyl)cyclopropyl)methyl)(cyclopropyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1308815-47-5
tert-butyl cyclopropyl((1-(4-nitrophenyl)cyclopropyl)methyl)carbamate

: 1308815-49-7
tert-butyl ((1-(4-aminophenyl)cyclopropyl)methyl)(cyclopropyl)carbamate

Guidance literature:: With ammonium formate; palladium on carbon; In methanol; at 60 ℃; for 1h;

Reference yield:

: 23348-99-4
1-(4-nitrophenyl)cyclopropane-1-carboxylic acid

: 1308815-49-7
tert-butyl ((1-(4-aminophenyl)cyclopropyl)methyl)(cyclopropyl)carbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine; methyl chloroformate / tetrahydrofuran / 0 - 10 °C / Inert atmosphere

1.2: 1 h / 0 °C

2.1: triethylamine / dichloromethane / 1 h / 0 - 5 °C

3.1: sodium hydrogencarbonate / acetonitrile / 5 h / 20 - 70 °C

4.1: ethyl acetate / 4 h / 20 °C

5.1: ammonium formate / palladium on carbon / methanol / 1 h / 60 °C

With ammonium formate; sodium hydrogencarbonate; triethylamine; methyl chloroformate; palladium on carbon; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetonitrile;

Reference yield:

: 23349-00-0
1-(4-nitrophenyl)-hydroxymethylcyclopropane

: 1308815-49-7
tert-butyl ((1-(4-aminophenyl)cyclopropyl)methyl)(cyclopropyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 1 h / 0 - 5 °C

2: sodium hydrogencarbonate / acetonitrile / 5 h / 20 - 70 °C

3: ethyl acetate / 4 h / 20 °C

4: ammonium formate / palladium on carbon / methanol / 1 h / 60 °C

With ammonium formate; sodium hydrogencarbonate; triethylamine; palladium on carbon; In methanol; dichloromethane; ethyl acetate; acetonitrile;