trans-cinnamoylsulfamoyl chloride

Base Information

• Chemical Name: trans-cinnamoylsulfamoyl chloride
• CAS No.: 53684-35-8
• Molecular Formula: C₉H₈ClNO₃S
• Molecular Weight: 245.686
• Mol file: 53684-35-8.mol

Synonyms:trans-cinnamoylsulfamoyl chloride

Chemical Property of trans-cinnamoylsulfamoyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-cinnamoylsulfamoyl chloride

There total 3 articles about trans-cinnamoylsulfamoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

isocyanate de chlorosulfonyle (1189-71-5) + Cinnamic acid (621-82-9) → trans-cinnamoylsulfamoyl chloride (53684-35-8)

Guidance literature:

In acetonitrile; at 22 - 39 ℃; for 1h;

DOI:10.1016/S0040-4020(01)89685-X

Reference yield:

isocyanate de chlorosulfonyle (1189-71-5) + (E)-3-phenylacrylic acid (140-10-3) → trans-cinnamoylsulfamoyl chloride (53684-35-8)

Guidance literature:

Reference yield:

→ trans-cinnamoylsulfamoyl chloride (53684-35-8)

Guidance literature:

N-Chlorsulfonylimino-trimethylsilylester (6), 2-Phenylethanol;

DOI:10.1021/jo00893a009

upstream raw materials:

isocyanate de chlorosulfonyle

(E)-3-phenylacrylic acid

Cinnamic acid

Downstream raw materials:

cinnamic nitrile

Refernces