(((1R,4S)-2,2-dibromo-1-methyl-4-(prop-1-en-2-yl)cyclohexyl)oxy)(isopropyl)dimethylsilane

Base Information

Chemical Name:(((1R,4S)-2,2-dibromo-1-methyl-4-(prop-1-en-2-yl)cyclohexyl)oxy)(isopropyl)dimethylsilane
CAS No.:1431302-65-6
Molecular Formula:C₁₅H₂₈Br₂OSi
Molecular Weight:412.28
Hs Code.:

Synonyms:(((1R,4S)-2,2-dibromo-1-methyl-4-(prop-1-en-2-yl)cyclohexyl)oxy)(isopropyl)dimethylsilane

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Chemical Property of (((1R,4S)-2,2-dibromo-1-methyl-4-(prop-1-en-2-yl)cyclohexyl)oxy)(isopropyl)dimethylsilane

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Technology Process of (((1R,4S)-2,2-dibromo-1-methyl-4-(prop-1-en-2-yl)cyclohexyl)oxy)(isopropyl)dimethylsilane

There total 5 articles about (((1R,4S)-2,2-dibromo-1-methyl-4-(prop-1-en-2-yl)cyclohexyl)oxy)(isopropyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1431302-67-8
N'-((2R,5S)-2-((isopropyldimethylsilyl)oxy)-2-methyl-5-(prop-1-en-2-yl)cyclohexylidene)-4-methylbenzenesulfonohydrazide

: 1431302-65-6
(((1R,4S)-2,2-dibromo-1-methyl-4-(prop-1-en-2-yl)cyclohexyl)oxy)(isopropyl)dimethylsilane

Guidance literature:: With n-butyllithium; copper(ll) bromide; In tetrahydrofuran; hexane; tert-butyl alcohol; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol400754e

Reference yield:

: 288264-99-3,7086-80-8
(2R,5S)-2-hydroxy-2-methyl-5-(prop-1-en-2-yl)cyclohexanone

: 1431302-65-6
(((1R,4S)-2,2-dibromo-1-methyl-4-(prop-1-en-2-yl)cyclohexyl)oxy)(isopropyl)dimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: 2,6-dimethylpyridine / dichloromethane / -78 - 20 °C / Inert atmosphere

2: methanol / 5 h / 20 °C

3: n-butyllithium; copper(ll) bromide / tetrahydrofuran; hexane; tert-butyl alcohol / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; n-butyllithium; copper(ll) bromide; In tetrahydrofuran; methanol; hexane; dichloromethane; tert-butyl alcohol;
DOI:10.1021/ol400754e

Reference yield:

: 203719-53-3
(-)-limonene oxide

: 1431302-65-6
(((1R,4S)-2,2-dibromo-1-methyl-4-(prop-1-en-2-yl)cyclohexyl)oxy)(isopropyl)dimethylsilane

Guidance literature:: Multi-step reaction with 5 steps

1: potassium phosphate / aq. phosphate buffer / 32 h / 20 °C / pH 3.1

2: 2-iodoxybenzoic acid / ethyl acetate / 16 h / Reflux

3: 2,6-dimethylpyridine / dichloromethane / -78 - 20 °C / Inert atmosphere

4: methanol / 5 h / 20 °C

5: n-butyllithium; copper(ll) bromide / tetrahydrofuran; hexane; tert-butyl alcohol / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; potassium phosphate; n-butyllithium; 2-iodoxybenzoic acid; copper(ll) bromide; In tetrahydrofuran; methanol; aq. phosphate buffer; hexane; dichloromethane; ethyl acetate; tert-butyl alcohol;
DOI:10.1021/ol400754e