Technology Process of C32H40(2)H3NO4
There total 7 articles about C32H40(2)H3NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium deuteride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 19h;
DOI:10.1002/jlcr.595
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 51 percent / NaOH; tetra-n-butylammonium hydrogen sulphate; benzyltrimethylammonium chloride / CH2Cl2; H2O / 192 h / 20 °C
2: 38 percent / Cs2CO3 / dimethylformamide / 5 h / 60 - 80 °C
3: 100 percent / i-Pr2EtN / tetrahydrofuran / 60 °C
4: 87 percent / LiAlD4 / tetrahydrofuran / 19 h / 0 - 20 °C
With
sodium hydroxide; lithium aluminium deuteride; tetra(n-butyl)ammonium hydrogensulfate; benzyltrimethylammonium chloride; caesium carbonate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/jlcr.595
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 51 percent / NaOH; tetra-n-butylammonium hydrogen sulphate; benzyltrimethylammonium chloride / CH2Cl2; H2O / 192 h / 20 °C
2: 38 percent / Cs2CO3 / dimethylformamide / 5 h / 60 - 80 °C
3: 100 percent / i-Pr2EtN / tetrahydrofuran / 60 °C
4: 87 percent / LiAlD4 / tetrahydrofuran / 19 h / 0 - 20 °C
With
sodium hydroxide; lithium aluminium deuteride; tetra(n-butyl)ammonium hydrogensulfate; benzyltrimethylammonium chloride; caesium carbonate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/jlcr.595
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