(R)-tert-butyl 1-methyl-1-[4-methylcyclohex-3-en-1-yl]ethylcarbamate

Base Information

• Chemical Name: (R)-tert-butyl 1-methyl-1-[4-methylcyclohex-3-en-1-yl]ethylcarbamate
• CAS No.: 774214-70-9
• Molecular Formula: C₁₅H₂₇NO₂
• Molecular Weight: 253.385
• Mol file: 774214-70-9.mol

Synonyms:(R)-tert-butyl 1-methyl-1-[4-methylcyclohex-3-en-1-yl]ethylcarbamate

Chemical Property of (R)-tert-butyl 1-methyl-1-[4-methylcyclohex-3-en-1-yl]ethylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (R)-tert-butyl 1-methyl-1-[4-methylcyclohex-3-en-1-yl]ethylcarbamate

There total 1 articles about (R)-tert-butyl 1-methyl-1-[4-methylcyclohex-3-en-1-yl]ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

di-tert-butyl dicarbonate (24424-99-5) + (4R)-4-(1-amino-1-methylethyl)-1-methylcyclohexene (67931-03-7) → (R)-tert-butyl 1-methyl-1-[4-methylcyclohex-3-en-1-yl]ethylcarbamate (774214-70-9)

Guidance literature:

With pyridine; In dichloromethane;

DOI:10.1071/CH03158

Reference yield: 50.0%

(R)-tert-butyl 1-methyl-1-[4-methylcyclohex-3-en-1-yl]ethylcarbamate (774214-70-9) → tert-butyl 1-[(1R,3S,4S)-3,4-dibromo-4-cyclohexyl]-1-methylethylcarbamate

Guidance literature:

With N-Bromosuccinimide; In acetone; for 19h;

DOI:10.1071/CH03158

Reference yield: 37.0%

(R)-tert-butyl 1-methyl-1-[4-methylcyclohex-3-en-1-yl]ethylcarbamate (774214-70-9) + mercury(II) diacetate (1600-27-7) → (1RS,5SR)-5-{1-[(tert-butoxycarbonyl)amino]-1-methylethyl}-2-methylcyclohex-2-en-1-yl acetate

Guidance literature:

(R)-tert-butyl 1-methyl-1-[4-methylcyclohex-3-en-1-yl]ethylcarbamate; mercury(II) diacetate; In dichloromethane; for 168h;

With sodium hydroxide; sodium tetrahydroborate; In dichloromethane; at -5 ℃; for 4h;

DOI:10.1071/CH03158

upstream raw materials:

di-tert-butyl dicarbonate

(4R)-4-(1-amino-1-methylethyl)-1-methylcyclohexene