(1,10-Phenanthroline)copper(II) Dichloride

Base Information

• Chemical Name: (1,10-Phenanthroline)copper(II) Dichloride
• CAS No.: 14783-09-6
• Molecular Formula: C12H8 Cl2 Cu N2
• Molecular Weight: 314.661
• Hs Code.: 29339900
• Mol file: 14783-09-6.mol

Synonyms:AKOS025394381;(1,10-Phenanthroline)copper(II) Dichloride;D3891

Chemical Property of (1,10-Phenanthroline)copper(II) Dichloride

Chemical Property:

• Vapor Pressure: 3.38E-05mmHg at 25°C
• Melting Point: 295 °C
• Boiling Point: 365.1°C at 760 mmHg
• Flash Point: 164.8°C
• PSA: 25.78000
• LogP: 4.15950
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 312.936051
• Heavy Atom Count: 17
• Complexity: 183

Purity/Quality:

97% ^*data from raw suppliers

Dichloro(1,10-phenanthroline)copper(II) ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22-37/38-41-36/37/38
• Safety Statements: 26-39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC2=C(C3=C(C=CC=N3)C=C2)N=C1.[Cl-].[Cl-].[Cu+2]
• Uses: Catalyst for:Oxidative carbonylation of methanolCyclohexane and toluene oxidationSelective oxidation of tetralin

Technology Process of (1,10-Phenanthroline)copper(II) Dichloride

There total 10 articles about (1,10-Phenanthroline)copper(II) Dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

chloro-trimethyl-silane (75-77-4) + Cu(1,10-phenanthroline)(3-n-nonylcatecholate) (73704-41-3) → dichloro(1,10-phenanthroline) copper(II) (14783-09-6)

Guidance literature:

With oxygen; In ethanol; water; the starting complex is dissolved in abs. ethanol, then addn. of H2O, O2is then slowly bubbled through the soln. for 6 h; the mixt. is evapd., residue is dissolved in diethyl ether, pptd. with (CH3)3SiCl;

Reference yield: 87.0%

1,10-Phenanthroline (66-71-7) + copper(II) choride dihydrate → dichloro(1,10-phenanthroline) copper(II) (14783-09-6)

Guidance literature:

In methanol; at 20 ℃; for 1h;

DOI:10.1002/anie.202016548

Reference yield: 78.0%

1,10-Phenanthroline (66-71-7) + copper dichloride → dichloro(1,10-phenanthroline) copper(II) (14783-09-6)

Guidance literature:

In ethanol;

DOI:10.1016/j.ica.2018.12.011

upstream raw materials:

1,10-phenanthroline hydrate

1,10-Phenanthroline

chloro-trimethyl-silane

Cu(1,10-phenanthroline)(3-n-nonylcatecholate)

Downstream raw materials:

{(1,10-phenanthroline)Cu(OC₆H₄-2-OH)2}

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