4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-methoxyphenoxy}ethyl)morpholine

Base Information

Chemical Name:4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-methoxyphenoxy}ethyl)morpholine
CAS No.:956222-36-9
Molecular Formula:C₂₀H₂₂ClN₅O₃
Molecular Weight:415.879
Hs Code.:

Synonyms:4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-methoxyphenoxy}ethyl)morpholine

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Chemical Property of 4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-methoxyphenoxy}ethyl)morpholine

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Technology Process of 4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-methoxyphenoxy}ethyl)morpholine

There total 4 articles about 4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-methoxyphenoxy}ethyl)morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₂₅N₃SO₅

: 106-47-8
4-chloro-aniline

: 956222-36-9
4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-methoxyphenoxy}ethyl)morpholine

Guidance literature:: 4-chloro-aniline; With hydrogenchloride; sodium nitrate; In ethanol; water;

C₂₀H₂₅N₃SO₅; With pyridine; In ethanol; water; at -15 - 20 ℃; for 0.75h; Further stages.;
DOI:10.1021/ol7017328

Reference yield:

: 2-methoxy-4-(2-morpholinoethoxy)benzaldehyde

: 956222-36-9
4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-methoxyphenoxy}ethyl)morpholine

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol / 1.5 h

2.1: sodium nitrate; hydrochloric acid / H₂O; ethanol

2.2: 2.8 g / pyridine / H₂O; ethanol / 0.75 h / -15 - 20 °C

With hydrogenchloride; sodium nitrate; In ethanol; water;
DOI:10.1021/ol7017328

Reference yield:

: 18278-34-7
4-hydroxy-2-methoxybenzaldehyde

: 956222-36-9
4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-methoxyphenoxy}ethyl)morpholine

Guidance literature:: Multi-step reaction with 3 steps

1.1: K₂CO₃ / dimethylformamide / 21 h / 50 °C

2.1: ethanol / 1.5 h

3.1: sodium nitrate; hydrochloric acid / H₂O; ethanol

3.2: 2.8 g / pyridine / H₂O; ethanol / 0.75 h / -15 - 20 °C

With hydrogenchloride; sodium nitrate; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ol7017328