4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-isopropoxyphenoxy}ethyl)morpholine

Base Information

Chemical Name:4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-isopropoxyphenoxy}ethyl)morpholine
CAS No.:956222-37-0
Molecular Formula:C₂₂H₂₆ClN₅O₃
Molecular Weight:443.933
Hs Code.:

Synonyms:4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-isopropoxyphenoxy}ethyl)morpholine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-isopropoxyphenoxy}ethyl)morpholine

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Technology Process of 4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-isopropoxyphenoxy}ethyl)morpholine

There total 6 articles about 4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-isopropoxyphenoxy}ethyl)morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-30-9
2-iodo-propane

: C₁₉H₂₀N₅O₃Cl

: 956222-37-0
4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-isopropoxyphenoxy}ethyl)morpholine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 23h;
DOI:10.1021/ol7017328

Reference yield:

: C₂₀H₂₅N₃SO₅

: 956222-37-0
4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-isopropoxyphenoxy}ethyl)morpholine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium nitrate; hydrochloric acid / H₂O; ethanol

1.2: 2.8 g / pyridine / H₂O; ethanol / 0.75 h / -15 - 20 °C

2.1: BBr₃ / CH₂Cl₂ / -78 - 20 °C

3.1: 98 mg / K₂CO₃ / dimethylformamide / 23 h / 50 °C

With hydrogenchloride; sodium nitrate; boron tribromide; potassium carbonate; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol7017328

Reference yield:

: 956222-36-9
4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-methoxyphenoxy}ethyl)morpholine

: 956222-37-0
4-(2-{4-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]-3-isopropoxyphenoxy}ethyl)morpholine

Guidance literature:: Multi-step reaction with 2 steps

1: BBr₃ / CH₂Cl₂ / -78 - 20 °C

2: 98 mg / K₂CO₃ / dimethylformamide / 23 h / 50 °C

With boron tribromide; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol7017328