2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-1-phenyl-4,7-octanedione

Base Information

Chemical Name:2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-1-phenyl-4,7-octanedione
CAS No.:875918-19-7
Molecular Formula:C₂₄H₂₇NO₆
Molecular Weight:425.481
Hs Code.:

Synonyms:2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-1-phenyl-4,7-octanedione

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Chemical Property of 2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-1-phenyl-4,7-octanedione

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Technology Process of 2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-1-phenyl-4,7-octanedione

There total 3 articles about 2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-1-phenyl-4,7-octanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-5-Benzyloxycarbonylamino-3-hydroxy-2-(2-oxo-propyl)-6-phenyl-hexanoic acid methyl ester

: 875918-19-7
2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-1-phenyl-4,7-octanedione

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃;
DOI:10.1002/ejoc.200500387

Reference yield:

: 105-45-3
acetoacetic acid methyl ester

: 875918-19-7
2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-1-phenyl-4,7-octanedione

Guidance literature:: Multi-step reaction with 2 steps

1.1: Et₂Zn / CH₂Cl₂ / 0.67 h / 0 °C

1.2: Et₂Zn / CH₂Cl₂ / 1 h / 0 °C

2.1: 1.9 g / PCC / CH₂Cl₂ / 20 °C

With diethylzinc; pyridinium chlorochromate; In dichloromethane;
DOI:10.1002/ejoc.200500387

Reference yield:

: 868670-42-2
((S)-1-Benzyl-3-oxo-propyl)-carbamic acid benzyl ester

: 875918-19-7
2-[(benzyloxycarbonyl)amino]-5-(methoxycarbonyl)-1-phenyl-4,7-octanedione

Guidance literature:: Multi-step reaction with 2 steps

1.1: Et₂Zn / CH₂Cl₂ / 0.67 h / 0 °C

1.2: Et₂Zn / CH₂Cl₂ / 1 h / 0 °C

2.1: 1.9 g / PCC / CH₂Cl₂ / 20 °C

With diethylzinc; pyridinium chlorochromate; In dichloromethane;
DOI:10.1002/ejoc.200500387