N₁-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)propyl)-N₈-(3-hydroxypropyl)-3,6-di(prop-1-ynyl)pyrene-1,8-dicarboxamide

Base Information

• Chemical Name: N₁-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)propyl)-N₈-(3-hydroxypropyl)-3,6-di(prop-1-ynyl)pyrene-1,8-dicarboxamide
• CAS No.: 1196794-25-8
• Molecular Formula: C₅₁H₄₆N₂O₆
• Molecular Weight: 782.936

Synonyms:N₁-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)propyl)-N₈-(3-hydroxypropyl)-3,6-di(prop-1-ynyl)pyrene-1,8-dicarboxamide

Chemical Property of N₁-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)propyl)-N₈-(3-hydroxypropyl)-3,6-di(prop-1-ynyl)pyrene-1,8-dicarboxamide

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Technology Process of N₁-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)propyl)-N₈-(3-hydroxypropyl)-3,6-di(prop-1-ynyl)pyrene-1,8-dicarboxamide

There total 1 articles about N₁-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)propyl)-N₈-(3-hydroxypropyl)-3,6-di(prop-1-ynyl)pyrene-1,8-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

3,6-bis-(1-propyn-1-yl)pyrene-1,8-dicarboxylic acid (1196794-24-7) + propan-1-ol-3-amine (156-87-6) + (4,4'-dimethoxytrityl)oxypropan-1-amine (184241-29-0) → N1-(3-(bis(4-methoxyphenyl)(phenyl)methoxy)propyl)-N8-(3-hydroxypropyl)-3,6-di(prop-1-ynyl)pyrene-1,8-dicarboxamide (1196794-25-8)

Guidance literature:

3,6-bis-(1-propyn-1-yl)pyrene-1,8-dicarboxylic acid; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;

(4,4'-dimethoxytrityl)oxypropan-1-amine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

propan-1-ol-3-amine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

DOI:10.1002/anie.200903251

upstream raw materials:

3,6-bis-(1-propyn-1-yl)pyrene-1,8-dicarboxylic acid

propan-1-ol-3-amine

(4,4'-dimethoxytrityl)oxypropan-1-amine

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